5,5-bis(benzoylsulfanylmethyl)imidazolidine-2,4-dione

Base Information

• Chemical Name: 5,5-bis(benzoylsulfanylmethyl)imidazolidine-2,4-dione
• CAS No.: 142979-93-9
• Molecular Formula: C₁₉H₁₆N₂O₄S₂
• Molecular Weight: 400.479
• Mol file: 142979-93-9.mol

Synonyms:5,5-bis(benzoylsulfanylmethyl)imidazolidine-2,4-dione;5,5-Bis((benzoylthio)methyl)-2,4-imidazolidinedione;5,5-Bis[(benzoylthio)methyl]-2,4-imidazolidinedione;5,5diPhCOSMe2 hydantoin

Chemical Property of 5,5-bis(benzoylsulfanylmethyl)imidazolidine-2,4-dione

Chemical Property:

• Boiling Point: °Cat760mmHg
• Flash Point: °C
• PSA: 149.92000
• Density: 1.361g/cm³
• LogP: 2.62770

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 5,5-bis(benzoylsulfanylmethyl)imidazolidine-2,4-dione

There total 2 articles about 5,5-bis(benzoylsulfanylmethyl)imidazolidine-2,4-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 36.0%

benzoyl chloride (98-88-4) + 5,5-bis(mercaptomethyl)-2,4-imidazolidinedione (142979-79-1) → 5,5-bis<(benzoylthio)methyl>-2,4-imidazolidinedione (142979-93-9)

Guidance literature:

With pyridine; Ambient temperature;

DOI:10.1021/jm00097a014

Reference yield:

5,5-bis<<(phenylmethyl)thio>methyl>-2,4-imidazolidinedione (32418-95-4) → 5,5-bis<(benzoylthio)methyl>-2,4-imidazolidinedione (142979-93-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 46 percent / NH₃ liq., Na / 0.17 h

2: 36 percent / pyridine / Ambient temperature

With pyridine; ammonia; sodium;

DOI:10.1021/jm00097a014

upstream raw materials:

benzoyl chloride

5,5-bis(mercaptomethyl)-2,4-imidazolidinedione

5,5-bis<<(phenylmethyl)thio>methyl>-2,4-imidazolidinedione