Piperidine, 4-(diphenylmethylene)-1-(methylsulfonyl)-

Base Information

Chemical Name:Piperidine, 4-(diphenylmethylene)-1-(methylsulfonyl)-
CAS No.:916976-31-3
Molecular Formula:C19H21NO2S
Molecular Weight:327.447
Hs Code.:
DSSTox Substance ID:DTXSID90475647
Nikkaji Number:J2.386.091K
Wikidata:Q82306306

Synonyms:Piperidine, 4-(diphenylmethylene)-1-(methylsulfonyl)-;916976-31-3;DTXSID90475647

Suppliers and Price of Piperidine, 4-(diphenylmethylene)-1-(methylsulfonyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of Piperidine, 4-(diphenylmethylene)-1-(methylsulfonyl)-

Chemical Property:

XLogP3:3.7
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:3
Exact Mass:327.12930009
Heavy Atom Count:23
Complexity:490

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CS(=O)(=O)N1CCC(=C(C2=CC=CC=C2)C3=CC=CC=C3)CC1

Technology Process of Piperidine, 4-(diphenylmethylene)-1-(methylsulfonyl)-

There total 10 articles about Piperidine, 4-(diphenylmethylene)-1-(methylsulfonyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 515154-31-1
4-benzoyl-1-methanesulphonylpiperidine

: phenylmagnesium bromide

: 916976-31-3
4-benzhydrylidene-1-methanesulfonyl-piperidine

Guidance literature:: 4-benzoyl-1-methanesulphonylpiperidine; phenylmagnesium bromide; In tetrahydrofuran; at -78 ℃;

With boron trifluoride diethyl etherate; In dichloromethane; at 0 ℃;
DOI:10.1016/j.tetlet.2006.11.072

Reference yield:

: (1-methanesulfonylpiperidin-4-yl)diphenylmethanol

: 916976-31-3
4-benzhydrylidene-1-methanesulfonyl-piperidine

Guidance literature:: With boron trifluoride diethyl etherate; In dichloromethane; at 20 ℃;
DOI:10.1016/j.tetlet.2006.09.068

Reference yield:

: 515154-31-1
4-benzoyl-1-methanesulphonylpiperidine

: 916976-31-3
4-benzhydrylidene-1-methanesulfonyl-piperidine

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran / -78 °C

2: BF₃*OEt₂ / CH₂Cl₂ / 20 °C

With boron trifluoride diethyl etherate; In tetrahydrofuran; dichloromethane;
DOI:10.1016/j.tetlet.2006.09.068