9H-Thioxanthen-9-one, 6-hydroxy-1-[[2-[(2-hydroxyethyl)amino]ethyl]amino]-4-methyl-

Base Information

Chemical Name:9H-Thioxanthen-9-one, 6-hydroxy-1-[[2-[(2-hydroxyethyl)amino]ethyl]amino]-4-methyl-
CAS No.:80568-46-3
Molecular Formula:C₁₈H₂₀N₂O₃S
Molecular Weight:344.434
Hs Code.:
NSC Number:327395
DSSTox Substance ID:DTXSID10419523
ChEMBL ID:CHEMBL72775

Synonyms:NSC327395;80568-46-3;CHEMBL72775;DTXSID10419523;NSC-327395;9H-Thioxanthen-9-one, 6-hydroxy-1-[[2-[(2-hydroxyethyl)amino]ethyl]amino]-4-methyl-

Suppliers and Price of 9H-Thioxanthen-9-one, 6-hydroxy-1-[[2-[(2-hydroxyethyl)amino]ethyl]amino]-4-methyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of 9H-Thioxanthen-9-one, 6-hydroxy-1-[[2-[(2-hydroxyethyl)amino]ethyl]amino]-4-methyl-

Chemical Property:

Vapor Pressure:8.16E-17mmHg at 25°C
Boiling Point:631.5°Cat760mmHg
Flash Point:335.7°C
Density:1.366g/cm³
XLogP3:1.7
Hydrogen Bond Donor Count:4
Hydrogen Bond Acceptor Count:6
Rotatable Bond Count:6
Exact Mass:344.11946368
Heavy Atom Count:24
Complexity:437

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC1=C2C(=C(C=C1)NCCNCCO)C(=O)C3=C(S2)C=C(C=C3)O

Technology Process of 9H-Thioxanthen-9-one, 6-hydroxy-1-[[2-[(2-hydroxyethyl)amino]ethyl]amino]-4-methyl-

There total 5 articles about 9H-Thioxanthen-9-one, 6-hydroxy-1-[[2-[(2-hydroxyethyl)amino]ethyl]amino]-4-methyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 27139-97-5
2-bromo-4-chloro-1-methyl-benzene

: 80568-46-3
6-Hydroxy-1-[2-(2-hydroxy-ethylamino)-ethylamino]-4-methyl-thioxanthen-9-one

Guidance literature:: Multi-step reaction with 4 steps

1: 25.3 g / K₂CO₃, KI, Cu bronze / dimethylformamide / 18 h / Heating

2: 5.0 g / conc. H₂SO₄ / 90 h / Heating

3: HI, acetic acid / 2 h / Heating

4: 1.0 g / pyridine / 16 h / Heating

With pyridine; copper bronze; sulfuric acid; hydrogen iodide; potassium carbonate; acetic acid; potassium iodide; In N,N-dimethyl-formamide;
DOI:10.1021/jm00345a006

Reference yield:

: 80568-44-1
2-mercapto-4-methoxybenzoic acid

: 80568-46-3
6-Hydroxy-1-[2-(2-hydroxy-ethylamino)-ethylamino]-4-methyl-thioxanthen-9-one

Guidance literature:: Multi-step reaction with 4 steps

1: 25.3 g / K₂CO₃, KI, Cu bronze / dimethylformamide / 18 h / Heating

2: 5.0 g / conc. H₂SO₄ / 90 h / Heating

3: HI, acetic acid / 2 h / Heating

4: 1.0 g / pyridine / 16 h / Heating

With pyridine; copper bronze; sulfuric acid; hydrogen iodide; potassium carbonate; acetic acid; potassium iodide; In N,N-dimethyl-formamide;
DOI:10.1021/jm00345a006

Reference yield:

: 60666-41-3
1-chloro-6-methoxy-4-methylthioxanthenone

: 80568-46-3
6-Hydroxy-1-[2-(2-hydroxy-ethylamino)-ethylamino]-4-methyl-thioxanthen-9-one

Guidance literature:: Multi-step reaction with 2 steps

1: HI, acetic acid / 2 h / Heating

2: 1.0 g / pyridine / 16 h / Heating

With pyridine; hydrogen iodide; acetic acid;
DOI:10.1021/jm00345a006