1H-Isoindol-1-one, 5-bromo-2,3-dihydro-2-phenyl-

Base Information

Chemical Name:1H-Isoindol-1-one, 5-bromo-2,3-dihydro-2-phenyl-
CAS No.:918330-02-6
Molecular Formula:C14H10BrNO
Molecular Weight:288.143
Hs Code.:

Synonyms:5-bromo-2-phenylisoindolin-1-one;5-bromo-2-phenyl-2,3-dihydroisoindol-1-one;1H-Isoindol-1-one,5-bromo-2,3-dihydro-2-phenyl;

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1H-Isoindol-1-one, 5-bromo-2,3-dihydro-2-phenyl-

Chemical Property:

PSA：20.31000
LogP:3.67450

Purity/Quality:

Safty Information:

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Technology Process of 1H-Isoindol-1-one, 5-bromo-2,3-dihydro-2-phenyl-

There total 5 articles about 1H-Isoindol-1-one, 5-bromo-2,3-dihydro-2-phenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.61%

: 62-53-3
aniline

: 78471-43-9
methyl 4-bromo-2-(bromomethyl)benzoate

: 918330-02-6
5-bromo-2-phenylisoindolin-1-one

Guidance literature:: at 40 ℃; for 0.0833333h;

Reference yield:

: 99548-55-7
4-bromo-2-methyl-benzoic acid methyl ester

: 918330-02-6
5-bromo-2-phenylisoindolin-1-one

Guidance literature:: Multi-step reaction with 3 steps

1: N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile) / 18 h / 80 °C / Inert atmosphere

2: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 10 - 35 °C

3: trifluoroacetic acid / acetonitrile / 0.5 h / 80 °C

With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In tetrahydrofuran; acetonitrile;