N-methylphenylacetohydroxamic acid

Base Information

Chemical Name:N-methylphenylacetohydroxamic acid
CAS No.:72229-75-5
Molecular Formula:C9H11 N O2
Molecular Weight:165.192
Hs Code.:
Mol file:72229-75-5.mol

Synonyms:N-(2-Phenylacetyl)-N-methylhydroxylamine;N-Hydroxy-N-methyl-2-phenylacetamide; N-Hydroxy-N-methylphenylacetamide; NSC646163

Suppliers and Price of N-methylphenylacetohydroxamic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of N-methylphenylacetohydroxamic acid

Chemical Property:

Vapor Pressure:0.000499mmHg at 25°C
Boiling Point:300.4°C at 760 mmHg
Flash Point:135.5°C
PSA：40.54000
Density:1.174g/cm³
LogP:1.07670

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of N-methylphenylacetohydroxamic acid

There total 2 articles about N-methylphenylacetohydroxamic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 4229-44-1
N-methylhydroxyamine hydrochloride

: 103-80-0
phenylacetyl chloride

: 72229-75-5
N-Hydroxy-N-methyl-2-phenylacetamide

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 1h;
DOI:10.1039/a909903d

Reference yield:

: 103-82-2
phenylacetic acid

: 72229-75-5
N-Hydroxy-N-methyl-2-phenylacetamide

Guidance literature:: Multi-step reaction with 2 steps

1: oxalyl chloride / CH₂Cl₂ / Ambient temperature

2: Et₃N / CH₂Cl₂ / 1 h / Ambient temperature

With oxalyl dichloride; triethylamine; In dichloromethane;

Reference yield: 88.0%

: 13734-36-6
N-(tert-butoxycarbonyl)sarcosine

: 72229-75-5
N-Hydroxy-N-methyl-2-phenylacetamide

: tert-butyl methyl{2-[(N-methyl-2-phenylacetamido)oxy]-2-oxoethyl}carbamate

Guidance literature:: With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In dichloromethane; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1055/s-0040-1706660