Technology Process of Propanoic acid, 2,2-dimethyl-,
5-[(1-phenyl-1H-tetrazol-5-yl)sulfonyl]pentyl ester
There total 5 articles about Propanoic acid, 2,2-dimethyl-,
5-[(1-phenyl-1H-tetrazol-5-yl)sulfonyl]pentyl ester which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
ammonium molybdate tetrahydrate; dihydrogen peroxide;
In
tetrahydrofuran;
at 20 ℃;
DOI:10.1016/j.tet.2006.09.019
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 84 percent / pyridine / CH2Cl2 / 10 - 20 °C
2: 92 percent / N-bromosuccinimide; triphenylphosphine / CH2Cl2 / 0 - 20 °C
3: 97 percent / anhydrous potassium carbonate / acetone / 19 h / 20 - 40 °C
4: 99 percent / hydrogen peroxide; ammonium heptamolybdate(VI) tetrahydrate / tetrahydrofuran; various solvent(s) / 20 °C
With
pyridine; N-Bromosuccinimide; ammonium molybdate tetrahydrate; dihydrogen peroxide; potassium carbonate; triphenylphosphine;
In
tetrahydrofuran; dichloromethane; acetone;
DOI:10.1016/j.tet.2006.09.019
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 84 percent / pyridine / CH2Cl2 / 10 - 20 °C
2: 92 percent / N-bromosuccinimide; triphenylphosphine / CH2Cl2 / 0 - 20 °C
3: 97 percent / anhydrous potassium carbonate / acetone / 19 h / 20 - 40 °C
4: 99 percent / hydrogen peroxide; ammonium heptamolybdate(VI) tetrahydrate / tetrahydrofuran; various solvent(s) / 20 °C
With
pyridine; N-Bromosuccinimide; ammonium molybdate tetrahydrate; dihydrogen peroxide; potassium carbonate; triphenylphosphine;
In
tetrahydrofuran; dichloromethane; acetone;
DOI:10.1016/j.tet.2006.09.019