1-Silanaphthalene, 1-(1,1-dimethylethyl)-1-[[(1R,2S,5R)-5-methyl-2-(1-methylethyl)cyclohex yl]oxy]-1,2,3,4-tetrahydro-

Base Information

Chemical Name:1-Silanaphthalene, 1-(1,1-dimethylethyl)-1-[[(1R,2S,5R)-5-methyl-2-(1-methylethyl)cyclohex yl]oxy]-1,2,3,4-tetrahydro-
CAS No.:919513-42-1
Molecular Formula:C₂₃H₃₈OSi
Molecular Weight:358.64
Hs Code.:

Synonyms:

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Chemical Property of 1-Silanaphthalene, 1-(1,1-dimethylethyl)-1-[[(1R,2S,5R)-5-methyl-2-(1-methylethyl)cyclohex yl]oxy]-1,2,3,4-tetrahydro-

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MSDS Files:: SDS file from LookChem

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Technology Process of 1-Silanaphthalene, 1-(1,1-dimethylethyl)-1-[[(1R,2S,5R)-5-methyl-2-(1-methylethyl)cyclohex yl]oxy]-1,2,3,4-tetrahydro-

There total 6 articles about 1-Silanaphthalene, 1-(1,1-dimethylethyl)-1-[[(1R,2S,5R)-5-methyl-2-(1-methylethyl)cyclohex yl]oxy]-1,2,3,4-tetrahydro- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 919513-39-6
rac-1-tert-butyl-1,2,3,4-tetrahydro-1-silanaphthalene

: 919513-42-1
(SiR)-1-tert-butyl-1-[(1R,2S,5R)-1-menthyloxy]-1,2,3,4-tetrahydro-1-silanaphthalene

Guidance literature:: Multi-step reaction with 2 steps

1.1: Cl₂ / CCl₄ / 0.07 h / 0 °C

2.1: KH / tetrahydrofuran / 1 h / Heating

2.2: 2.50 g / tetrahydrofuran / 4 h / Heating

With chlorine; potassium hydride; In tetrahydrofuran; tetrachloromethane;
DOI:10.1002/adsc.200606071

Reference yield:

: 919513-39-6
rac-1-tert-butyl-1,2,3,4-tetrahydro-1-silanaphthalene

: 919513-42-1
(SiS)-1-tert-butyl-1-[(1R,2S,5R)-1-menthyloxy]-1,2,3,4-tetrahydro-1-silanaphthalene

Guidance literature:: Multi-step reaction with 2 steps

1.1: Cl₂ / CCl₄ / 0.07 h / 0 °C

2.1: KH / tetrahydrofuran / 1 h / Heating

2.2: 2.24 g / tetrahydrofuran / 4 h / Heating

With chlorine; potassium hydride; In tetrahydrofuran; tetrachloromethane;
DOI:10.1002/adsc.200606071

Reference yield:

: 1075-28-1
1-bromo-2-(3-bromopropyl)benzene

: 919513-42-1
(SiR)-1-tert-butyl-1-[(1R,2S,5R)-1-menthyloxy]-1,2,3,4-tetrahydro-1-silanaphthalene

Guidance literature:: Multi-step reaction with 3 steps

1.1: magnesium turnings; 1,2-dibromoethane / tetrahydrofuran / 24 h / Heating

1.2: 45 percent / LiAlH₄ / tetrahydrofuran / 20 h / Heating

2.1: Cl₂ / CCl₄ / 0.07 h / 0 °C

3.1: KH / tetrahydrofuran / 1 h / Heating

3.2: 2.50 g / tetrahydrofuran / 4 h / Heating

With chlorine; potassium hydride; magnesium; ethylene dibromide; In tetrahydrofuran; tetrachloromethane; 1.1: Grignard reaction;
DOI:10.1002/adsc.200606071