Carbamodithioic acid, (2-(ethenyloxy)ethyl)-, ethyl ester

Base Information

• Chemical Name: Carbamodithioic acid, (2-(ethenyloxy)ethyl)-, ethyl ester
• CAS No.: 126560-43-8
• Molecular Formula: C₇H₁₃NOS₂
• Molecular Weight: 191.318
• DSSTox Substance ID: DTXSID30155214
• Wikidata: Q83023013
• Mol file: 126560-43-8.mol

Synonyms:126560-43-8;Ethyl (2-(ethenyloxy)ethyl)carbamodithioate;Carbamodithioic acid, (2-(ethenyloxy)ethyl)-, ethyl ester;BRN 3537570;Ethyl (2-(vinyloxy)ethyl)carbamodithioate;DTXSID30155214;LS-50805

Chemical Property of Carbamodithioic acid, (2-(ethenyloxy)ethyl)-, ethyl ester

Chemical Property:

• Vapor Pressure: 0.00929mmHg at 25°C
• Boiling Point: 265.2°Cat760mmHg
• Flash Point: 114.2°C
• Density: 1.103g/cm³
• XLogP3: 2.1
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 6
• Exact Mass: 191.04385639
• Heavy Atom Count: 11
• Complexity: 128

Purity/Quality:

85.0-99.8% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCSC(=S)NCCOC=C

Technology Process of Carbamodithioic acid, (2-(ethenyloxy)ethyl)-, ethyl ester

There total 4 articles about Carbamodithioic acid, (2-(ethenyloxy)ethyl)-, ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.2%

ethyl bromide (74-96-4) + Potassium N-<(2-vinyloxy)ethyl>dithiocarbamate (97006-62-7) → ethyl N-2-vinyloxyethylcarbamodithioate (126560-43-8)

Guidance literature:

In dimethyl sulfoxide; at 30 - 35 ℃; for 1h;

DOI:10.1007/BF00766868

Reference yield: 96.0%

Potassium N-<(2-vinyloxy)ethyl>dithiocarbamate (97006-62-7) → ethyl N-2-vinyloxyethylcarbamodithioate (126560-43-8)

Guidance literature:

In dimethyl sulfoxide; at 30 - 35 ℃; for 1h;

Reference yield: 86.0%

carbon disulfide (75-15-0,12122-00-8) + ethyl bromide (74-96-4) + 2-aminoethyl vinyl ether (7336-29-0) → ethyl N-2-vinyloxyethylcarbamodithioate (126560-43-8)

Guidance literature:

carbon disulfide; 2-aminoethyl vinyl ether; With triethylamine; In benzene; at 0 - 5 ℃;

ethyl bromide; In benzene; at 20 ℃;

DOI:10.1134/S1070363216060074

upstream raw materials:

ethyl bromide

Potassium N-<(2-vinyloxy)ethyl>dithiocarbamate

2-(vinyloxy)ethyl isothiocyanate

ethanethiol