1,4-Acridinedione, 3-bromo-2-methoxy-

Base Information

Chemical Name:1,4-Acridinedione, 3-bromo-2-methoxy-
CAS No.:77282-37-2
Molecular Formula:C₁₄H₈BrNO₃
Molecular Weight:318.126
Hs Code.:2933990090
DSSTox Substance ID:DTXSID30228013
Wikidata:Q83107882
Mol file:77282-37-2.mol

Synonyms:1,4-Acridinedione, 3-bromo-2-methoxy-;BRN 5566015;77282-37-2;3-Bromo-2-methoxy-1,4-acridinedione;Bromo-3 methoxy-2 acridinedione-1,4 [French];Bromo-3 methoxy-2 acridinedione-1,4;DTXSID30228013

Suppliers and Price of 1,4-Acridinedione, 3-bromo-2-methoxy-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
1,4-ACRIDINEDIONE, 3-BROMO-2-METHOXY- 95.00%
5MG
$ 504.46

Total 3 raw suppliers

Chemical Property of 1,4-Acridinedione, 3-bromo-2-methoxy-

Chemical Property:

Vapor Pressure:6.66E-09mmHg at 25°C
Melting Point:223 °C
Boiling Point:467.2°C at 760 mmHg
PKA:-3.95±0.20(Predicted)
Flash Point:236.3°C
PSA：56.26000
Density:1.7g/cm³
LogP:2.86670
XLogP3:3.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:1
Exact Mass:316.96876
Heavy Atom Count:19
Complexity:460

Purity/Quality:

99% ^*data from raw suppliers

1,4-ACRIDINEDIONE, 3-BROMO-2-METHOXY- 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=C(C(=O)C2=NC3=CC=CC=C3C=C2C1=O)Br

Technology Process of 1,4-Acridinedione, 3-bromo-2-methoxy-

There total 11 articles about 1,4-Acridinedione, 3-bromo-2-methoxy- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 77282-16-7
methoxy-2 acridinedione-1,4

: 77282-37-2
bromo-3 methoxy-2 acridinedione-1,4

Guidance literature:: With bromine; In chloroform; for 24h; Ambient temperature;

Reference yield:

: 16492-13-0
9-chloro-2-methoxyacridine

: 77282-37-2
bromo-3 methoxy-2 acridinedione-1,4

Guidance literature:: Multi-step reaction with 6 steps

1: 1.) hydrogen, potassium hydroxide; 2.) ferrous chloride, oxygen / 1.) Raney-nickel / 1.) r.t., benzene, methanol; 2.) 60 deg C, 4 h

2: 96 percent / KNO₃ / aq. H₂SO₄ / 1 h / -2 - 0 °C

3: 1.) aluminium amalgame; 2.) oxygen / 1.) ethanol, 95 deg C, 1 h; 2.) 8 h

4: 1.) sodium nitrite, p-sulfanilic acid, sodium acetate; 3.) sodium dithionite, 2.5 percent sodium hydroxide / 1.) acetic acid, -2 deg C, 1 h; 2.) 33 percent aq. acetic acid, 0 deg C, 15 min; 3.) 1 h

5: 1.5 M sulfuric acid, potassium dichromate / CHCl₃

6: 66 percent / bromine / CHCl₃ / 24 h / Ambient temperature

With potassium dichromate; potassium hydroxide; sodium hydroxide; sodium dithionite; aluminium amalgam; sulfuric acid; hydrogen; bromine; oxygen; sodium acetate; potassium nitrate; iron(II) chloride; sodium nitrite; 4-aminobenzene sulfonic acid; nickel; In chloroform; sulfuric acid;

Reference yield:

: 86-38-4
6,9-dichloro-2-methoxyacridine

: 77282-37-2
bromo-3 methoxy-2 acridinedione-1,4

Guidance literature:: Multi-step reaction with 6 steps

1: 1.) hydrogen, potassium hydroxide; 2.) ferrous chloride, oxygen / 1.) Raney-nickel / 1.) r.t., benzene, methanol; 2.) 60 deg C, 4 h

2: 96 percent / KNO₃ / aq. H₂SO₄ / 1 h / -2 - 0 °C

3: 1.) aluminium amalgame; 2.) oxygen / 1.) ethanol, 95 deg C, 1 h; 2.) 8 h

4: 1.) sodium nitrite, p-sulfanilic acid, sodium acetate; 3.) sodium dithionite, 2.5 percent sodium hydroxide / 1.) acetic acid, -2 deg C, 1 h; 2.) 33 percent aq. acetic acid, 0 deg C, 15 min; 3.) 1 h

5: 1.5 M sulfuric acid, potassium dichromate / CHCl₃

6: 66 percent / bromine / CHCl₃ / 24 h / Ambient temperature

With potassium dichromate; potassium hydroxide; sodium hydroxide; sodium dithionite; aluminium amalgam; sulfuric acid; hydrogen; bromine; oxygen; sodium acetate; potassium nitrate; iron(II) chloride; sodium nitrite; 4-aminobenzene sulfonic acid; nickel; In chloroform; sulfuric acid;