1,6-Heptadien-4-ol, 4-(2-phenylethenyl)-

Base Information

• Chemical Name: 1,6-Heptadien-4-ol, 4-(2-phenylethenyl)-
• CAS No.: 92581-12-9
• Molecular Formula: C15H18O
• Molecular Weight: 214.307
• DSSTox Substance ID: DTXSID90388642
• Mol file: 92581-12-9.mol

Synonyms:1,6-Heptadien-4-ol, 4-(2-phenylethenyl)-;92581-12-9;DTXSID90388642

Chemical Property of 1,6-Heptadien-4-ol, 4-(2-phenylethenyl)-

Chemical Property:

• XLogP3: 3.7
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 6
• Exact Mass: 214.135765193
• Heavy Atom Count: 16
• Complexity: 236

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C=CCC(CC=C)(C=CC1=CC=CC=C1)O

Technology Process of 1,6-Heptadien-4-ol, 4-(2-phenylethenyl)-

There total 11 articles about 1,6-Heptadien-4-ol, 4-(2-phenylethenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

tris(allyl)aluminum (18854-66-5) + Cinnamoyl chloride (102-92-1,17082-09-6) → 4-trans-styryl-hepta-1,6-dien-4-ol (92581-12-9)

Guidance literature:

In tetrahydrofuran; at 20 ℃; for 0.5h;

DOI:10.1016/j.tetlet.2007.07.008

Reference yield: 96.0%

Methyl cinnamate (103-26-4,1754-62-7) + allyl bromide (106-95-6) → 4-trans-styryl-hepta-1,6-dien-4-ol (92581-12-9)

Guidance literature:

With bis(cyclopentadienyl)titanium dichloride; magnesium; In tetrahydrofuran; at 20 ℃;

DOI:10.1016/j.tetlet.2010.02.144

Reference yield: 96.0%

(E)-cinnamoyl azide (26829-64-1) + allyl bromide (106-95-6) → 4-trans-styryl-hepta-1,6-dien-4-ol (92581-12-9)

Guidance literature:

allyl bromide; With samarium; In tetrahydrofuran; at 20 ℃;

(E)-cinnamoyl azide; In tetrahydrofuran; at 20 ℃; for 0.0833333h;

upstream raw materials:

diethyl ether

(E)-1-methylpropyl cinnamate

allylmagnesium bromide

allyl bromide