4H-1,2,4-Triazol-4-amine, 3,5-bis(4-methoxyphenyl)-

Base Information

Chemical Name:4H-1,2,4-Triazol-4-amine, 3,5-bis(4-methoxyphenyl)-
CAS No.:93016-27-4
Molecular Formula:C16H16N4O2
Molecular Weight:296.329
Hs Code.:
DSSTox Substance ID:DTXSID40445855
Nikkaji Number:J1.086.628F
Wikidata:Q82264391

Synonyms:4H-1,2,4-Triazol-4-amine, 3,5-bis(4-methoxyphenyl)-;93016-27-4;DTXSID40445855;3,5-bis(4-methoxyphenyl)-4-amino-1,2,4-triazole;3,5-Bis(4-methoxyphenyl)-4H-1,2,4-triazole-4-amine

Suppliers and Price of 4H-1,2,4-Triazol-4-amine, 3,5-bis(4-methoxyphenyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4H-1,2,4-Triazol-4-amine, 3,5-bis(4-methoxyphenyl)-

Chemical Property:

XLogP3:2.4
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:4
Exact Mass:296.12732577
Heavy Atom Count:22
Complexity:309

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=CC=C(C=C1)C2=NN=C(N2N)C3=CC=C(C=C3)OC

Technology Process of 4H-1,2,4-Triazol-4-amine, 3,5-bis(4-methoxyphenyl)-

There total 4 articles about 4H-1,2,4-Triazol-4-amine, 3,5-bis(4-methoxyphenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 74-83-9
methyl bromide

: 223645-69-0
4,4’-(4-amino-4H-1,2,4-triazole-3,5-diyl)diphenol

: 93016-27-4
3,5-bis(4-methoxyphenyl)-4-amino-1,2,4-triazole

Guidance literature:: With potassium carbonate; In acetone; for 20h; Reflux;
DOI:10.1016/j.tet.2016.06.013

Reference yield: 86.0%

: 874-90-8
4-methoxybenzonitrile

: 93016-27-4
3,5-bis(4-methoxyphenyl)-4-amino-1,2,4-triazole

Guidance literature:: With hydrazine dihydrochloride; hydrazine hydrate; In ethylene glycol; at 130 ℃;
DOI:10.1002/jhet.5570360123

Reference yield:

: 123-11-5
4-methoxy-benzaldehyde

: 93016-27-4
3,5-bis(4-methoxyphenyl)-4-amino-1,2,4-triazole

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / hydroxylamine hydrochloride; N-methyl-2-pyrrolidinone / 0.05 h / 200 °C / microwave irradiation

2: hydrazine dihydrochloride; hydrazine monohydrate / ethane-1,2-diol / 0.2 h / 160 °C / microwave irradiation

With 1-methyl-pyrrolidin-2-one; hydrazine dihydrochloride; hydroxylamine hydrochloride; hydrazine hydrate; In ethylene glycol;
DOI:10.3987/COM-02-9584