Benzenesulfonamide, N-(2-benzoyl-4-bromophenyl)-4-methyl-

Base Information

Chemical Name:Benzenesulfonamide, N-(2-benzoyl-4-bromophenyl)-4-methyl-
CAS No.:94579-32-5
Molecular Formula:C20H16BrNO3S
Molecular Weight:430.322
Hs Code.:
DSSTox Substance ID:DTXSID20361948

Synonyms:94579-32-5;Benzenesulfonamide, N-(2-benzoyl-4-bromophenyl)-4-methyl-;CBMicro_000876;SCHEMBL29148;DTXSID20361948;SMSF0008252;STK534990;AKOS000669303;CB02507;BIM-0000932.P001;SR-01000422782;SR-01000422782-1;Z57157526;N~1~-(2-benzoyl-4-bromophenyl)-4-methyl-1-benzenesulfonamide;N-[4-bromo-2-(phenylcarbonyl)phenyl]-4-methylbenzenesulfonamide

Suppliers and Price of Benzenesulfonamide, N-(2-benzoyl-4-bromophenyl)-4-methyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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Total 0 raw suppliers

Chemical Property of Benzenesulfonamide, N-(2-benzoyl-4-bromophenyl)-4-methyl-

Chemical Property:

XLogP3:5.4
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:5
Exact Mass:429.00343
Heavy Atom Count:26
Complexity:574

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC=C(C=C1)S(=O)(=O)NC2=C(C=C(C=C2)Br)C(=O)C3=CC=CC=C3

Technology Process of Benzenesulfonamide, N-(2-benzoyl-4-bromophenyl)-4-methyl-

There total 6 articles about Benzenesulfonamide, N-(2-benzoyl-4-bromophenyl)-4-methyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₆H₁₇BrN₂O₄S

: 100-58-3
phenylmagnesium bromide

: 94579-32-5
2-N-Tosylamino-5-bromobenzophenone

Guidance literature:: In tetrahydrofuran; at 20 ℃; for 18h; Inert atmosphere;
DOI:10.1002/chem.201202606

Reference yield:

: 39859-36-4
2-amino-5-bromobenzophenone

: 98-59-9
p-toluenesulfonyl chloride

: 94579-32-5
2-N-Tosylamino-5-bromobenzophenone

Guidance literature:: With pyridine;

Reference yield:

: 98-59-9
p-toluenesulfonyl chloride

: 94579-32-5
2-N-Tosylamino-5-bromobenzophenone

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / tetrahydrofuran; water / 3 h / 20 °C / Inert atmosphere

2: 4-methyl-morpholine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 18 h / 0 - 20 °C / Inert atmosphere

3: tetrahydrofuran / 18 h / 20 °C / Inert atmosphere

With 4-methyl-morpholine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In tetrahydrofuran; dichloromethane; water;
DOI:10.1002/chem.201202606