Technology Process of Furan, 2,3-diphenyl-
There total 13 articles about Furan, 2,3-diphenyl- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
gold(III) tribromide; silver trifluoromethanesulfonate;
In
water;
at 20 ℃;
for 2h;
Reagent/catalyst;
Darkness;
Sealed tube;
DOI:10.1021/ol403402h
- Guidance literature:
-
(3-methoxyprop-1-yn-1-yl)benzene;
With
n-butyllithium;
In
tetrahydrofuran;
at -40 ℃;
for 1h;
Inert atmosphere;
benzaldehyde;
In
tetrahydrofuran;
at -40 ℃;
for 1.5h;
Inert atmosphere;
With
pyridine; gold(I) chloride;
In
dichloromethane;
at 20 ℃;
for 38h;
Overall yield = 75 percent; Overall yield = 200 mg; regioselective reaction;
Inert atmosphere;
DOI:10.1055/s-0040-1705958
- Guidance literature:
-
(3-methoxyprop-1-yn-1-yl)benzene;
With
n-butyllithium;
In
tetrahydrofuran; hexane;
at -78 ℃;
Inert atmosphere;
benzaldehyde;
In
tetrahydrofuran; hexane;
at -78 ℃;
Inert atmosphere;
With
potassium carbonate; silver nitrate;
In
acetonitrile;
at 20 ℃;
for 19h;
regioselective reaction;
Inert atmosphere;
Darkness;
DOI:10.1055/s-0040-1705958