BENZYLP-TOLYLSULFONE

Base Information

• Chemical Name: BENZYLP-TOLYLSULFONE
• CAS No.: 5395-20-0
• Molecular Formula: C14H14O2S
• Molecular Weight: 246.33
• Mol file: 5395-20-0.mol

Synonyms:1-(Benzylsulfonyl)-4-methylbenzene;Benzene, 1-methyl-4-[(phenylmethyl)sulfonyl]-;benzyl 4-methylphenyl sulfone;BENZYL P-TOLYL SULFONE;1-methyl-4-(benzylsulfonyl)benzene;1-methyl-4-phenylmethanesulfonyl-benzene;phenyl-p-toluenesulfonyl methane;4-methylphenyl benzyl sulfone;

Chemical Property of BENZYLP-TOLYLSULFONE

Chemical Property:

• Vapor Pressure: 3.56E-07mmHg at 25°C
• Boiling Point: 429.3°Cat760mmHg
• Flash Point: 264.5°C
• PSA: 42.52000
• Density: 1.183g/cm³
• LogP: 4.04970

Purity/Quality:

99% ^*data from raw suppliers

BENZYL P-TOLYL SULFONE Aldrich ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of BENZYLP-TOLYLSULFONE

There total 97 articles about BENZYLP-TOLYLSULFONE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

benzyl bromide (100-39-0) + sodium 4-methylbenzenesulfinate (824-79-3) → 1-methyl-4-(benzylsulfonyl)benzene (5395-20-0)

Guidance literature:

In 1,4-dioxane; water;

DOI:10.1016/j.tet.2014.02.024

Reference yield: 99.0%

1-benzylsulfanyl-4-methyl-benzene (5023-60-9) → 1-methyl-4-(benzylsulfonyl)benzene (5395-20-0)

Guidance literature:

With Oxone; aluminium trichloride; for 0.5h; Heating;

Reference yield: 99.0%

di(4-methyl)phenylthiosulfonate (2943-42-2) + benzyl bromide (100-39-0) → 1-methyl-4-(benzylsulfonyl)benzene (5395-20-0)

Guidance literature:

With 1,3,4,6,7,8-hexahydro-2H-pyrimido[1,2-a]pyrimidine; In tetrahydrofuran; at 65 ℃; for 16h; Reagent/catalyst; Temperature; Solvent; Sealed tube;

upstream raw materials:

benzaldehyde p-toluenesulfonylhydrazone

phenyl-(toluene-4-sulfonyl)-acetic acid

α-<(4-methylphenyl)sulfonyl>benzeneacetic acid ethyl ester

di(4-methyl)phenylthiosulfonate

Downstream raw materials:

1,1,2-triphenyl-2-(toluene-4-sulfonyl)-ethanol

1,1-Diphenyl-2-(4-phenylmethanesulfonyl-phenyl)-ethanol

1-(2,2-Bis-methylsulfanyl-1-phenyl-ethenesulfonyl)-4-methyl-benzene

1-Methyl-4-(1-phenyl-cyclopentanesulfonyl)-benzene