1,2-Ethenediol, 1,2-diphenyl-, dibenzoate

Base Information

Chemical Name:1,2-Ethenediol, 1,2-diphenyl-, dibenzoate
CAS No.:96276-54-9
Molecular Formula:C28H20O4
Molecular Weight:420.464
Hs Code.:

Synonyms:

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Chemical Property of 1,2-Ethenediol, 1,2-diphenyl-, dibenzoate

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Technology Process of 1,2-Ethenediol, 1,2-diphenyl-, dibenzoate

There total 2 articles about 1,2-Ethenediol, 1,2-diphenyl-, dibenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: Collman's reagent

: 98-88-4
benzoyl chloride

: 96276-54-9
1,2-diphenylethene-1,2-diyl dibenzoate

: 110098-08-3
(CO)3Fe(C₆H₅CCC₆H₅O)Fe(CO)3

: 134-81-6
benzil

Guidance literature:: In tetrahydrofuran; byproducts: carbon monoxide, carbon dioxide; Na2Fe(CO)4*1.5C4H8O2 reacted with 2 molar equiv of PhCOCl in THF at 0°C under a nitrogen atmosphere for 24 h; after first 30 min IR spectrum showed the presence of the intermediate anion; evapd., hexane added, filtered, concn. of filtrate yielded crystals of diester, hexane soln. was chromd. (Al2O3, CH2Cl2-hexane), recrystd. from hexane-CH2Cl2 to give Fe-complex; benzil was detected by TLC and GC, gas atm. was analysed by IR spectroscopy;

Reference yield:

: 98-88-4
benzoyl chloride

: 134-81-6
benzil

: 96276-54-9
1,2-diphenylethene-1,2-diyl dibenzoate

Guidance literature:: benzil; With iodine; magnesium; In tetrahydrofuran; for 3.08333h; Inert atmosphere;

benzoyl chloride; In tetrahydrofuran; for 2h;