4-Propargyloxybenzoyl chloride

Base Information

Chemical Name:4-Propargyloxybenzoyl chloride
CAS No.:96327-77-4
Molecular Formula:C10H7ClO2
Molecular Weight:194.617
Hs Code.:
DSSTox Substance ID:DTXSID90541977
Nikkaji Number:J872.349D
Wikidata:Q82418472

Synonyms:4-propargyloxybenzoyl chloride;96327-77-4;SCHEMBL9718528;DTXSID90541977;NNYZPPIZGHMNOA-UHFFFAOYSA-N;4-[(Prop-2-yn-1-yl)oxy]benzoyl chloride

Suppliers and Price of 4-Propargyloxybenzoyl chloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 4-Propargyloxybenzoyl chloride

Chemical Property:

PSA：26.30000
LogP:2.07760
XLogP3:2.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:194.0134572
Heavy Atom Count:13
Complexity:220

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C#CCOC1=CC=C(C=C1)C(=O)Cl

Technology Process of 4-Propargyloxybenzoyl chloride

There total 4 articles about 4-Propargyloxybenzoyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 21926-55-6
4-(prop-2-ynyloxy)benzoic acid

: 96327-77-4
4-(prop-2-yn-1-yloxy)benzoyl chloride

Guidance literature:: With oxalyl dichloride; In acetonitrile; at 20 ℃; for 5h;
DOI:10.1002/ejoc.200600079

Reference yield:

: 99-76-3,156291-94-0
methyl 4-hydroxylbenzoate

: 96327-77-4
4-(prop-2-yn-1-yloxy)benzoyl chloride

Guidance literature:: Multi-step reaction with 3 steps

1: 96 percent / K₂CO₃ / toluene / 20 °C

2: 99 percent / NaOH / methanol / 20 °C

3: oxalyl chloride / acetonitrile / 5 h / 20 °C

With sodium hydroxide; oxalyl dichloride; potassium carbonate; In methanol; toluene; acetonitrile;
DOI:10.1002/ejoc.200600079