1,4-Diethyl-2,5-diiodobenzene

Base Information

Chemical Name:1,4-Diethyl-2,5-diiodobenzene
CAS No.:96802-17-4
Molecular Formula:C10H12I2
Molecular Weight:386.014
Hs Code.:2903999090
DSSTox Substance ID:DTXSID40540935
Wikidata:Q82417076
Mol file:96802-17-4.mol

Synonyms:1,4-diethyl-2,5-diiodobenzene;96802-17-4;SCHEMBL6510330;DTXSID40540935;CTWJTDSEKVBFMK-UHFFFAOYSA-N;AKOS015967244

Suppliers and Price of 1,4-Diethyl-2,5-diiodobenzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
1,4-DIETHYL-2,5-DIIODO-BENZENE 95.00%
5MG
$ 499.49

Total 3 raw suppliers

Chemical Property of 1,4-Diethyl-2,5-diiodobenzene

Chemical Property:

Vapor Pressure:0.00015mmHg at 25°C
Boiling Point:342.4oC at 760 mmHg
Flash Point:163.4oC
PSA：0.00000
Density:1.937g/cm3
LogP:4.02060
XLogP3:4.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:2
Exact Mass:385.90285
Heavy Atom Count:12
Complexity:120

Purity/Quality:: 1,4-DIETHYL-2,5-DIIODO-BENZENE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCC1=CC(=C(C=C1I)CC)I

Technology Process of 1,4-Diethyl-2,5-diiodobenzene

There total 2 articles about 1,4-Diethyl-2,5-diiodobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 105-05-5
1,4-diethylbenzene

: 96802-17-4
1,4-diiodo-2,5-diethylbenzene

Guidance literature:: With sulfuric acid; iodine; periodic acid; In water; acetic acid; at 95 ℃; for 24h;
DOI:10.1002/1521-3765(20011203)7:23<5118::AID-CHEM5118>3.0.CO;2-1

Reference yield:

: 937-30-4
4-ethylacetophenone

: 96802-17-4
1,4-diiodo-2,5-diethylbenzene

Guidance literature:: Multi-step reaction with 2 steps

1: 77 percent / aq. HCl; H₂ / Pd/C / ethanol / 50 °C / 3102.97 Torr

2: 56 percent / I₂; H₅IO₆*2H₂O; H₂SO₄ / acetic acid; H₂O / 22 h / 100 °C

With hydrogenchloride; sulfuric acid; hydrogen; iodine; periodic acid; palladium on activated charcoal; In ethanol; water; acetic acid;
DOI:10.5555/ol007036g

Reference yield: 96.0%

: 96802-17-4
1,4-diiodo-2,5-diethylbenzene

: 1066-54-2
trimethylsilylacetylene

: 339175-65-4
1,4-bis(trimethylsilylethynyl)-2,5-diethylbenzene

Guidance literature:: With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; diisopropylamine; In toluene; at 20 ℃; Inert atmosphere;
DOI:10.1016/j.tet.2010.05.016