[4,5-DICHLORO-6-OXO-1(6H)-PYRIDAZINYL]METHYL ACETATE

Base Information

• Chemical Name: [4,5-DICHLORO-6-OXO-1(6H)-PYRIDAZINYL]METHYL ACETATE
• CAS No.: 97137-15-0
• Molecular Formula: C7H6Cl2N2O3
• Molecular Weight: 237.04
• Hs Code.: 2933998090
• Mol file: 97137-15-0.mol

Synonyms:1-Acetoxymethyl-4,5-dichlor-pyridazon;2-acetoxymethyl-4,5-dichloro-2H-pyridazin-3-one;

Chemical Property of [4,5-DICHLORO-6-OXO-1(6H)-PYRIDAZINYL]METHYL ACETATE

Chemical Property:

• PSA: 61.19000
• LogP: 1.07070

Purity/Quality:

99% ^*data from raw suppliers

(4,5-Dichloro-6-oxo-1,6-dihydropyridazin-1-yl)methylacetate tech ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of [4,5-DICHLORO-6-OXO-1(6H)-PYRIDAZINYL]METHYL ACETATE

There total 3 articles about [4,5-DICHLORO-6-OXO-1(6H)-PYRIDAZINYL]METHYL ACETATE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

acetyl chloride (75-36-5) + 4,5-dichloro-2-(hydroxymethyl)pyridazin-3(2H)-one (51355-97-6) → 1-acetoxymethyl-4,5-dichloropyridazin-6-one (97137-15-0)

Guidance literature:

With potassium carbonate; In acetone; for 10h; Ambient temperature;

DOI:10.1002/jhet.5570330205

Reference yield:

acetic acid (64-19-7,77671-22-8) + 4,5-dichloro-2-chloromethyl-pyridazin-3(2H)-one (51356-03-7) → 1-acetoxymethyl-4,5-dichloropyridazin-6-one (97137-15-0)

Guidance literature:

With potassium carbonate; Heating;

DOI:10.1002/jhet.5570360213

Reference yield:

→ 1-acetoxymethyl-4,5-dichloropyridazin-6-one (97137-15-0)

Guidance literature:

4,5-Dichlor-pyridazon, Essigsaeure-halogenmethylester (?);

upstream raw materials:

acetyl chloride

4,5-dichloro-2-(hydroxymethyl)pyridazin-3(2H)-one

acetic acid

4,5-dichloro-2-chloromethyl-pyridazin-3(2H)-one

Downstream raw materials:

1-(acetoxymethyl)-5-chloro-4-phenoxypyridazin-6-one

5-chloro-4-phenoxypyridazin-6-one

1-acetoxymethyl-5-chloro-4-(4-nitrophenoxy)pyridazin-6-one

5-chloro-4-(4-methoxyphenoxy)pyridazin-6-one