4-amino-6-(4-methoxybenzyl)-3-(methylsulfanyl)-1,2,4-triazin-5(4H)-one

Base Information

Chemical Name:4-amino-6-(4-methoxybenzyl)-3-(methylsulfanyl)-1,2,4-triazin-5(4H)-one
CAS No.:98515-39-0
Molecular Formula:C12H14N4O2S
Molecular Weight:278.33000
Hs Code.:
Mol file:98515-39-0.mol

Synonyms:4-Amino-6-(4-methoxy-benzyl)-3-methylsulfanyl-4H-[1,2,4]triazin-5-one;

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-amino-6-(4-methoxybenzyl)-3-(methylsulfanyl)-1,2,4-triazin-5(4H)-one

Chemical Property:

PSA：108.33000
LogP:1.25460

Purity/Quality:

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Technology Process of 4-amino-6-(4-methoxybenzyl)-3-(methylsulfanyl)-1,2,4-triazin-5(4H)-one

There total 4 articles about 4-amino-6-(4-methoxybenzyl)-3-(methylsulfanyl)-1,2,4-triazin-5(4H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 4-amino-5-oxo-4-thioxo-6-(p-methoxybenzyl)-2,3,4,5-tetrahydro-1,2,4-triazine

: 74-88-4
methyl iodide

: 98515-39-0
4-amino-6-(4-methoxybenzyl)-3-methylthio-4,5-dihydro-1,2,4-triazin-5-one

Guidance literature:: With sodium methylate; In methanol; at 20 ℃;
DOI:10.1081/NCN-200040663

Reference yield: 65.0%

: 98515-75-4
4-Amino-3-mercapto-6-(4-methoxy-benzyl)-4H-[1,2,4]triazin-5-one

: 74-88-4
methyl iodide

: 98515-39-0
4-amino-6-(4-methoxybenzyl)-3-methylthio-4,5-dihydro-1,2,4-triazin-5-one

Guidance literature:: With sodium methylate; In methanol; for 0.25h; Ambient temperature; Heating;

Reference yield:

: 57427-78-8
(4Z)-4-(4-methoxybenzylidene)-2-phenyl-oxazolin-5-one

: 98515-39-0
4-amino-6-(4-methoxybenzyl)-3-methylthio-4,5-dihydro-1,2,4-triazin-5-one

Guidance literature:: Multi-step reaction with 3 steps

1: KOH / H₂O / 6.5 h / Heating

2: acetic acid; H₂O / 0.17 h / Ambient temperature; Heating

3: 65 percent / CH₃ONa / methanol / 0.25 h / Ambient temperature; Heating

With potassium hydroxide; sodium methylate; In methanol; water; acetic acid;