Hydroxylamine, O,O'-1,3-propanediylbis-

Base Information

• Chemical Name: Hydroxylamine, O,O'-1,3-propanediylbis-
• CAS No.: 98627-69-1
• Molecular Formula: C3H10N2O2
• Molecular Weight: 106.125
• Mol file: 98627-69-1.mol

Synonyms:O,O'-propane-1,3-diyl-bis-hydroxylamine;hydroxylamine-O-[3-(aminooxy)propyl];1.3-Bis-aminooxy-propan;Hydroxylamine,O,O'-1,3-propanediylbis;1,3-bis-aminooxy-propane;1,3-diaminoxypropane;

Chemical Property of Hydroxylamine, O,O'-1,3-propanediylbis-

Chemical Property:

• PSA: 70.50000
• LogP: 0.55770

Purity/Quality:

99% ^*data from raw suppliers

1,3-Bis-aminooxypropane 98% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Description: 1,3-Bis-aminooxy propane is a samll molecule PEG reagent containing two aminooxy groups. It can react with an aldehyde to form an oxime bond. If a reductant is used, it will form a hydroxylamine linkage. Aminooxy compounds are very reactive and sensitive; they cannot be stored for long term. Immediate use (within 1 week) is highly recommended.

Technology Process of Hydroxylamine, O,O'-1,3-propanediylbis-

There total 3 articles about Hydroxylamine, O,O'-1,3-propanediylbis- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,3-bis(phthalimidooxy)propane (94212-54-1) → 1,3-diaminoxypropane (98627-69-1)

Guidance literature:

With hydrogen bromide; In acetic acid;

DOI:10.1021/jo01041a042

Reference yield:

N-hydroxyphthalimide (524-38-9) + 1,8-diazabicyclo[5.4.0]undec-7-ene (6674-22-2,83329-50-4) + 1,3-dibromo-propane (109-64-8) → 1,3-bis(phthalimidooxy)propane (94212-54-1) + 1,3-diaminoxypropane (98627-69-1)

Guidance literature:

In N,N-dimethyl-formamide;

Reference yield:

N-hydroxyphthalimide (524-38-9) + 1,3-dibromo-propane (109-64-8) → 1,3-diaminoxypropane (98627-69-1)

Guidance literature:

N-hydroxyphthalimide; 1,3-dibromo-propane;

With hydrazine hydrate;

DOI:10.1080/10426507.2018.1452228

upstream raw materials:

1,3-bis(phthalimidooxy)propane

N-hydroxyphthalimide

1,8-diazabicyclo[5.4.0]undec-7-ene

1,3-dibromo-propane

Downstream raw materials:

3,3'-dimethoxy-2,2'-[(1,3-propylene)dioxybis(nitrilomethylidyne)]diphenol

N,N′-bis(5-bromosalicylidenimino)-1,3-diaminopropane

4,4'-dichloro-2,2'-[(1,3-propylene)dioxybis(nitrilomethylidyne)]diphenol

4,4'-dinitro-2,2'-[(propylene-1,3-diyldioxy)bis(nitrilomethylidyne)]diphenol