Benzenemethanamine, a-methyl-N-(1-methyl-2-phenylethylidene)-, (S)-

Base Information

Chemical Name:Benzenemethanamine, a-methyl-N-(1-methyl-2-phenylethylidene)-, (S)-
CAS No.:133505-53-0
Molecular Formula:C17H19N
Molecular Weight:269.38132
Hs Code.:

Synonyms:: R-(N-BENZYL-A-METHYL-2-AMINO)-1-(4-METHOXYPHENYL)PROPANE;[(S)-2-(4-Methoxy-phenyl)-1-methyl-ethyl]-((S)-1-phenyl-ethyl)-amine;

Suppliers and Price of Benzenemethanamine, a-methyl-N-(1-methyl-2-phenylethylidene)-, (S)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 5 raw suppliers

Chemical Property of Benzenemethanamine, a-methyl-N-(1-methyl-2-phenylethylidene)-, (S)-

Chemical Property:

PSA：21.26000
LogP:4.36790

Purity/Quality:: 98%,99%, ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Benzenemethanamine, a-methyl-N-(1-methyl-2-phenylethylidene)-, (S)-

There total 3 articles about Benzenemethanamine, a-methyl-N-(1-methyl-2-phenylethylidene)-, (S)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 122-84-9
4-methoxybenzyl methyl ketone

: 2627-86-3
(S)-1-phenyl-ethylamine

: (R)-1-(4-methoxyphenyl)-N-((S)-1-phenylethyl)propan-2-amine

: 133505-53-0
(S)-1-(4-methoxyphenyl)-N-((S)-1-phenylethyl)propan-2-amine

Guidance literature:: With formic acid; Cp*IrCl((S)-N-(phenyl(pyridin-2-yl)methyl)methanesulfonamide)complex; In methanol; at 40 ℃; for 22h; Reagent/catalyst; Overall yield = 89 %; stereoselective reaction; Inert atmosphere;

Reference yield:

: 98-86-2
acetophenone

: (R)-1-(4-methoxyphenyl)-N-((S)-1-phenylethyl)propan-2-amine

: 133505-53-0
(S)-1-(4-methoxyphenyl)-N-((S)-1-phenylethyl)propan-2-amine

Guidance literature:: Multi-step reaction with 2 steps

1: Cp*IrCl((S)-N-(1-(pyridin-2-yl)ethyl)methanesulfonamide)complex; ammonium formate; acetic acid / methanol / 7 h / 60 °C / Inert atmosphere

2: Cp*IrCl((S)-N-(phenyl(pyridin-2-yl)methyl)methanesulfonamide)complex; formic acid / methanol / 22 h / 40 °C / Inert atmosphere

With formic acid; Cp*IrCl((S)-N-(1-(pyridin-2-yl)ethyl)methanesulfonamide)complex; Cp*IrCl((S)-N-(phenyl(pyridin-2-yl)methyl)methanesulfonamide)complex; ammonium formate; acetic acid; In methanol;