2-[(2E)-2-(4-methoxybenzylidene)hydrazinyl]-6-methylpyrimidin-4(1H)-one

Base Information

Chemical Name:2-[(2E)-2-(4-methoxybenzylidene)hydrazinyl]-6-methylpyrimidin-4(1H)-one
CAS No.:92023-96-6
Molecular Formula:C13H14 N4 O2
Molecular Weight:258.28
Hs Code.:

Synonyms:Benzaldehyde,4-methoxy-, (4-oxo-1,4-dihydro-6-methyl-2-pyrimidinyl)hydrazone (9CI);p-Anisaldehyde, (4-hydroxy-6-methyl-2-pyrimidinyl)hydrazone (6CI,7CI); NSC97973

Suppliers and Price of 2-[(2E)-2-(4-methoxybenzylidene)hydrazinyl]-6-methylpyrimidin-4(1H)-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 5 raw suppliers

Chemical Property of 2-[(2E)-2-(4-methoxybenzylidene)hydrazinyl]-6-methylpyrimidin-4(1H)-one

Chemical Property:

Vapor Pressure:0mmHg at 25°C
Boiling Point:410.2°Cat760mmHg
Flash Point:201.9°C
Density:1.25g/cm³

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2-[(2E)-2-(4-methoxybenzylidene)hydrazinyl]-6-methylpyrimidin-4(1H)-one

There total 6 articles about 2-[(2E)-2-(4-methoxybenzylidene)hydrazinyl]-6-methylpyrimidin-4(1H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 37893-08-6
2-hydrazino-6-methylpyrimidin-4(3H)-one

: 123-11-5
4-methoxy-benzaldehyde

: 92023-96-6
E-2-[2-(4-methoxybenzylidene)hydrazinyl]-6-methylpyrimidin-4-one

Guidance literature:: With acetic acid; Temperature; Reflux;
DOI:10.1016/j.bioorg.2020.103616

Reference yield:

: 56-04-2
2-mercapto-6-methylpyrimidin-4(3H)-one

: 92023-96-6
E-2-[2-(4-methoxybenzylidene)hydrazinyl]-6-methylpyrimidin-4-one

Guidance literature:: Multi-step reaction with 2 steps

1: hydrazine hydrate / water; butan-1-ol / Reflux

2: acetic acid / Reflux

With hydrazine hydrate; acetic acid; In water; butan-1-ol;
DOI:10.1016/j.bioorg.2020.103616

Reference yield:

: 6328-58-1
6-methyl-2-methylsulfanyl-3H-pyrimidin-4-one

: 92023-96-6
E-2-[2-(4-methoxybenzylidene)hydrazinyl]-6-methylpyrimidin-4-one

Guidance literature:: Multi-step reaction with 2 steps

1: hydrazine hydrate / isopropyl alcohol / Reflux

2: acetic acid / Reflux

With hydrazine hydrate; acetic acid; In isopropyl alcohol;
DOI:10.1016/j.bioorg.2020.103616