2-chloro-N-cyclohexylbenzamide

Base Information

Chemical Name:2-chloro-N-cyclohexylbenzamide
CAS No.:59507-54-9
Molecular Formula:C13H16ClNO
Molecular Weight:237.729
Hs Code.:2924299090
Mol file:59507-54-9.mol

Synonyms:Benzamide,N-bromo-2-chloro;2-Chlor-benzoesaeure-bromamid;2-chloro-N-cyclohexylbenzamide;o-Chlorbenzoylcyclohexylamid;2-Chlorbenzoesaeurecyclohexylamid;2-chloro-benzoic acid bromoamide;2-Chlor-N-brombenzamid;

Suppliers and Price of 2-chloro-N-cyclohexylbenzamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Aronis compounds
2-chloro-N-cyclohexylbenzamide
1mg
$ 12.00

American Custom Chemicals Corporation
2-CHLORO-N-CYCLOHEXYLBENZAMIDE 95.00%
5MG
$ 496.11

Total 7 raw suppliers

Chemical Property of 2-chloro-N-cyclohexylbenzamide

Chemical Property:

Vapor Pressure:3.95E-06mmHg at 25°C
Boiling Point:384.9°Cat760mmHg
Flash Point:186.6°C
PSA：29.10000
Density:1.17g/cm³
LogP:3.79340

Purity/Quality:

99% ^*data from raw suppliers

2-chloro-N-cyclohexylbenzamide ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2-chloro-N-cyclohexylbenzamide

There total 5 articles about 2-chloro-N-cyclohexylbenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 108-91-8,157973-60-9
cyclohexylamine

: 118-91-2
ortho-chlorobenzoic acid

: 59507-54-9
2-chloro-N-cyclohexylbenzamide

Guidance literature:: ortho-chlorobenzoic acid; With 1,3,5-trichloro-2,4,6-triazine; potassium carbonate; triphenylphosphine; at 20 ℃; for 0.166667h;

cyclohexylamine; at 20 ℃; for 0.333333h;
DOI:10.1039/c5ra10127a

Reference yield: 47.0%

: potassium (2-chlorophenyl)trifluoroborate

: 13144-62-2
2-(cyclohexylamino)-2-oxoacetic acid

: 59507-54-9
2-chloro-N-cyclohexylbenzamide

Guidance literature:: With dipotassium peroxodisulfate; palladium diacetate; silver nitrate; In water; dimethyl sulfoxide; acetonitrile; at 70 ℃; for 0.166667h;
DOI:10.1039/c1cc11635e

Reference yield:

: 118-91-2
ortho-chlorobenzoic acid

: 59507-54-9
2-chloro-N-cyclohexylbenzamide

Guidance literature:: Multi-step reaction with 2 steps

1: diphenyl phosphorochloridate, triethylamine / CH₂Cl₂ / 0.25 h / Ambient temperature

2: triethylamine / CH₂Cl₂ / Ambient temperature

With triethylamine; chlorophosphoric acid diphenyl ester; In dichloromethane;
DOI:10.1055/s-1982-29783