Hexahydro-4h-1,3-benzodioxine

Base Information

Chemical Name:Hexahydro-4h-1,3-benzodioxine
CAS No.:13309-99-4
Molecular Formula:C₈H₁₄O₂
Molecular Weight:142.198
Hs Code.:
NSC Number:193320,30529
DSSTox Substance ID:DTXSID90927934

Synonyms:13309-99-4;hexahydro-4h-1,3-benzodioxine;1,3-dioxadecalin;2931-14-8;NSC30529;1, hexahydro-, trans-;4H-1, hexahydro-, trans-;SCHEMBL7092351;DTXSID90927934;Hexahydro-2H,4H-1,3-benzodioxine;NSC-30529;NSC193320;AKOS024336485;NSC-193320

Suppliers and Price of Hexahydro-4h-1,3-benzodioxine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of Hexahydro-4h-1,3-benzodioxine

Chemical Property:

Vapor Pressure:0.364mmHg at 25°C
Boiling Point:205.1°Cat760mmHg
Flash Point:73.8°C
Density:1.011g/cm³
XLogP3:1.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:0
Exact Mass:142.099379685
Heavy Atom Count:10
Complexity:114

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1CCC2C(C1)COCO2

Technology Process of Hexahydro-4h-1,3-benzodioxine

There total 7 articles about Hexahydro-4h-1,3-benzodioxine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 110-83-8
cyclohexene

: 2931-14-8,13309-99-4,22267-92-1
(4ar,8at)-hexahydro-1,3-benzodioxine

Guidance literature:: With sulfuric acid; In water; at 70 ℃;

Reference yield:

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 4187-59-1,4187-60-4,27583-43-3,29569-80-0,51606-49-6,51606-50-9,69308-85-6,96553-66-1,106758-67-2
trans-2-hydroxymethylcyclohexanol

: 2931-14-8,13309-99-4,22267-92-1
(4ar,8at)-hexahydro-1,3-benzodioxine

Guidance literature:: With hydrogenchloride;
DOI:10.1021/ja01579a048

Reference yield:

: 609-69-8,1123-72-4,1654-66-6,1654-67-7,1655-00-1,1655-01-2,3749-17-5,17502-32-8,28131-61-5
(+/-)-(1R,2S)-cis-2-hydroxy-1-cyclohexanecarboxylic acid

: 2931-14-8,13309-99-4,22267-92-1
(4ar,8ac)-hexahydro-1,3-benzodioxine

Guidance literature:: Multi-step reaction with 2 steps

1: LiAlH₄; diethyl ether

2: water; sulfuric acid

With lithium aluminium tetrahydride; diethyl ether; sulfuric acid; water;
DOI:10.1021/ja01579a048