(NE)-N-[1-amino-3-(4-methoxy-N-methylanilino)propan-2-ylidene]hydroxylamine

Base Information

Chemical Name:(NE)-N-[1-amino-3-(4-methoxy-N-methylanilino)propan-2-ylidene]hydroxylamine
CAS No.:82740-35-0
Molecular Formula:C11H17N3O2
Molecular Weight:223.2716
Hs Code.:
NSC Number:266524
DSSTox Substance ID:DTXSID10422890

Synonyms:NSC266524;82740-35-0;DTXSID10422890;NSC-266524

Suppliers and Price of (NE)-N-[1-amino-3-(4-methoxy-N-methylanilino)propan-2-ylidene]hydroxylamine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of (NE)-N-[1-amino-3-(4-methoxy-N-methylanilino)propan-2-ylidene]hydroxylamine

Chemical Property:

Vapor Pressure:1.78E-07mmHg at 25°C
Boiling Point:410.5°Cat760mmHg
Flash Point:202.1°C
Density:1.14g/cm³
XLogP3:1.1
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:5
Exact Mass:223.132076794
Heavy Atom Count:16
Complexity:225

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CN(CC(=NO)CN)C1=CC=C(C=C1)OC
Isomeric SMILES:CN(C/C(=N/O)/CN)C1=CC=C(C=C1)OC

Technology Process of (NE)-N-[1-amino-3-(4-methoxy-N-methylanilino)propan-2-ylidene]hydroxylamine

There total 1 articles about (NE)-N-[1-amino-3-(4-methoxy-N-methylanilino)propan-2-ylidene]hydroxylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 82585-46-4
2-{2-[(E)-Hydroxyimino]-3-[(4-methoxy-phenyl)-methyl-amino]-propyl}-isoindole-1,3-dione

: 82740-35-0
1-Amino-3-[(4-methoxy-phenyl)-methyl-amino]-propan-2-one oxime

Guidance literature:: With hydrazine; In ethanol; at 40 ℃; for 22h; Yield given;
DOI:10.1021/jm00351a008

Reference yield: 75.0%

: 6506-86-1
ethyl (6-amino-4-chloro-5-nitropyridin-2-yl)carbamate

: 82740-35-0
1-Amino-3-[(4-methoxy-phenyl)-methyl-amino]-propan-2-one oxime

: 82585-58-8
(6-Amino-4-{2-[(E)-hydroxyimino]-3-[(4-methoxy-phenyl)-methyl-amino]-propylamino}-5-nitro-pyridin-2-yl)-carbamic acid ethyl ester

Guidance literature:: With triethylamine; In methanol; at 75 ℃; for 15h;
DOI:10.1021/jm00351a008

Reference yield:

: 82740-35-0
1-Amino-3-[(4-methoxy-phenyl)-methyl-amino]-propan-2-one oxime

: 82585-90-8
(5-amino-3-[(4-methoxy-phenyl)-methyl-amino]-methyl-1,2-dihydro-pyrido[3,4-b]pyrazin-7-yl)-carbamic acid ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent / Et₃N / methanol / 15 h / 75 °C

2: 73 percent / H₂ / Raney nickel / ethanol / 3 h / 760 Torr / Ambient temperature

With hydrogen; triethylamine; nickel; In methanol; ethanol;
DOI:10.1021/jm00351a008