trimethyl-[4-trimethylsilyl-2,3-bis(trimethylsilylmethyl)but-2-enyl]si lane

Base Information

Chemical Name:trimethyl-[4-trimethylsilyl-2,3-bis(trimethylsilylmethyl)but-2-enyl]si lane
CAS No.:64174-59-0
Molecular Formula:C₁₈H₄₄Si₄
Molecular Weight:372.889
Hs Code.:2931900090

Synonyms:tetrakis(trimethylsilylmethyl)ethylene;Tetrakis(trimethylsilylmethyl)ethen;Silane,(2,3-bis(trimethylsilyl)methyl)-2-butene-1,4-diyl)bis(trimethyl;

Suppliers and Price of trimethyl-[4-trimethylsilyl-2,3-bis(trimethylsilylmethyl)but-2-enyl]si lane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 3 raw suppliers

Chemical Property of trimethyl-[4-trimethylsilyl-2,3-bis(trimethylsilylmethyl)but-2-enyl]si lane

Chemical Property:

Vapor Pressure:0.00171mmHg at 25°C
Boiling Point:303.1°Cat760mmHg
Flash Point:101.4°C
PSA：0.00000
Density:0.807g/cm³
LogP:7.63580

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of trimethyl-[4-trimethylsilyl-2,3-bis(trimethylsilylmethyl)but-2-enyl]si lane

There total 4 articles about trimethyl-[4-trimethylsilyl-2,3-bis(trimethylsilylmethyl)but-2-enyl]si lane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

: 75-77-4
chloro-trimethyl-silane

: 30432-16-7
1,4-dibromo-2,3-bis-bromomethyl-but-2-ene

: 64174-59-0
Tetrakis(trimethylsilylmethyl)ethen

Guidance literature:: With sodium; potassium; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; 1.) room temperature, 2 h, 2.) ferlux, 2 h;
DOI:10.1021/ja00533a023

Reference yield:

: 64174-59-0
Tetrakis(trimethylsilylmethyl)ethen

: 64174-59-0
tetrakis(trimethylsilylmethyl)ethylene radical cation

Guidance literature:: With aluminium trichloride; In dichloromethane;
DOI:10.1021/ja00533a023

Reference yield:

: 30432-16-7
1,4-dibromo-2,3-bis-bromomethyl-but-2-ene

: 64174-59-0
tetrakis(trimethylsilylmethyl)ethylene radical cation

Guidance literature:: Multi-step reaction with 2 steps

1: 20 percent / sodium, potassium(trace) / tetrahydrofuran; hexamethylphosphoric acid triamide / 1.) room temperature, 2 h, 2.) ferlux, 2 h

2: AlCl₃ / CH₂Cl₂

With aluminium trichloride; sodium; potassium; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; dichloromethane;
DOI:10.1021/ja00533a023