[2-(methylsulfanyl)phenyl](diphenyl)phosphane

Base Information

Chemical Name:[2-(methylsulfanyl)phenyl](diphenyl)phosphane
CAS No.:14791-94-7
Molecular Formula:C19H17 P S
Molecular Weight:308.384
Hs Code.:
Mol file:14791-94-7.mol

Synonyms:Phosphine,[o-(methylthio)phenyl]diphenyl- (8CI); (o-Methylthiophenyl)diphenylphosphine;NSC 310398; [(2-Methylthio)phenyl]diphenylphosphine;o-(Diphenylphosphino)thioanisole

Suppliers and Price of [2-(methylsulfanyl)phenyl](diphenyl)phosphane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of [2-(methylsulfanyl)phenyl](diphenyl)phosphane

Chemical Property:

Vapor Pressure:1.26E-06mmHg at 25°C
Boiling Point:412.2°Cat760mmHg
Flash Point:203.1°C
Density:g/cm³

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of [2-(methylsulfanyl)phenyl](diphenyl)phosphane

There total 3 articles about [2-(methylsulfanyl)phenyl](diphenyl)phosphane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 19614-16-5
2-bromo-1-(methylsulfanyl)benzene

: 1079-66-9,74391-44-9
chloro-diphenylphosphine

: 14791-94-7
o-(diphenylphosphino)thioanisole

Guidance literature:: 2-bromo-1-(methylsulfanyl)benzene; With n-butyllithium; In diethyl ether; hexane; at -78 ℃; for 1h; Inert atmosphere; Schlenk technique;

chloro-diphenylphosphine; In diethyl ether; hexane; at -78 - 20 ℃; for 3h; Inert atmosphere; Schlenk technique;
DOI:10.1021/jacs.8b05957

Reference yield:

: 33775-94-9
2-(methylthio)iodobenzene

: 829-85-6
diphenylphosphane

: 14791-94-7
o-(diphenylphosphino)thioanisole

: bis(2-methylthiophenyl)diphenylphosphonium iodide

Guidance literature:: With 1,3-dicyano-5-fluoro-2,4,6-tris(diphenylamino)benzene; triethylamine; In acetonitrile; for 18h; Inert atmosphere; Glovebox; Sealed tube; Irradiation;
DOI:10.1002/chem.202002646