1,1-Dibutoxypropane

Base Information

• Chemical Name: 1,1-Dibutoxypropane
• CAS No.: 13002-10-3
• Molecular Formula: C11H24 O2
• Molecular Weight: 188.31
• Hs Code.: 2909199090
• Mol file: 13002-10-3.mol

Synonyms:Propionaldehyde,dibutyl acetal (6CI,7CI,8CI); Propane, 1,1-dibutoxy- (8CI)

Chemical Property of 1,1-Dibutoxypropane

Chemical Property:

• Vapor Pressure: 0.364mmHg at 25°C
• Boiling Point: 205.1°C at 760 mmHg
• Flash Point: 49.3°C
• PSA: 18.46000
• Density: 0.843g/cm³
• LogP: 3.35590

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1,1-Dibutoxypropane

There total 8 articles about 1,1-Dibutoxypropane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

Tributyl orthoformate (588-43-2) + triethylaluminum (97-93-8) → propionaldehyde dibutylacetal (13002-10-3)

Guidance literature:

In dichloromethane; at -20 - 20 ℃;

DOI:10.1023/A:1024433300486

Reference yield:

allyl n-butyl ether (3739-64-8) + butan-1-ol (71-36-3) → propionaldehyde dibutylacetal (13002-10-3)

Guidance literature:

tris(triphenylphosphine)ruthenium(II) chloride; at 120 ℃; for 3h;

DOI:10.1016/j.tetlet.2006.10.138

Reference yield:

allyl n-butyl ether (3739-64-8) + benzyl alcohol (100-51-6,185532-71-2) → butyl (1-propenyl) ether (7748-07-4) + propionaldehyde dibutylacetal (13002-10-3) + [(1-butoxypropoxy)methyl]benzene

Guidance literature:

tris(triphenylphosphine)ruthenium(II) chloride; at 120 ℃; for 3h;

DOI:10.1016/j.tetlet.2006.10.138

upstream raw materials:

1,1-dibutoxy-prop-2-en

propionaldehyde

butan-1-ol

Tributyl orthoformate

Downstream raw materials:

propionaldehyde