Dichloro(phenyl)phosphinetungsten pentacarbonyl

Base Information

Chemical Name:Dichloro(phenyl)phosphinetungsten pentacarbonyl
CAS No.:18461-46-6
Molecular Formula:C₁₁H₅Cl₂O₅PW
Molecular Weight:502.887
Hs Code.:
Mol file:18461-46-6.mol

Synonyms:

Suppliers and Price of Dichloro(phenyl)phosphinetungsten pentacarbonyl

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Dichloro(phenyl)phosphinetungsten pentacarbonyl

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Dichloro(phenyl)phosphinetungsten pentacarbonyl

There total 3 articles about Dichloro(phenyl)phosphinetungsten pentacarbonyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

: 82839-15-4
chlorophenylphosphine-pentacarbonyl-tungsten⁽⁰⁾=Chlorophenylphosphin-pentacarbonyl-wolfram⁽⁰⁾

: 61300-75-2
phenylphosphine pentacarbonyltungsten⁽⁰⁾

: 18461-46-6
PhPCl₂W(CO)5

Guidance literature:: With aluminium trichloride; In dichloromethane; W complex treated with AlCl3 in CH2Cl2 at room temp. under Ar for 3 h, mixture hydrolyzed; evapn., chromy. (SiO2, hexane);

Reference yield:

: 14040-11-0
tungsten hexacarbonyl

: 18461-46-6
PhPCl₂W(CO)5

Guidance literature:: Multi-step reaction with 2 steps

1: acetonitrile

2: tetrahydrofuran

In tetrahydrofuran; acetonitrile;

Reference yield:

: 15096-68-1
pentacarbonyl(acetonitrile)tungsten

: 644-97-3
Dichlorophenylphosphine

: 18461-46-6
PhPCl₂W(CO)5

Guidance literature:: In tetrahydrofuran; addn. of org. compd. to W-complex in THF, heating (overnight, 50°C); solvent evapn., addn. of hexane, filtration;