1-bromo-4-[(4-nitrobenzyl)oxy]benzene

Base Information

• Chemical Name: 1-bromo-4-[(4-nitrobenzyl)oxy]benzene
• CAS No.: 6943-02-8
• Molecular Formula: C13H10BrNO3
• Molecular Weight: 308.131
• Hs Code.: 2909309090

Synonyms:p-Nitrobenzyl-p-bromphenylether;4-phenoxy-(4'-nitro)-benzylbromide;(4-bromo-phenyl)-(4-nitro-benzyl)-ether;1-bromo-4-[(4-nitrobenzyl)oxy]benzene;(4-Brom-phenyl)-(4-nitro-benzyl)-aether;

Chemical Property of 1-bromo-4-[(4-nitrobenzyl)oxy]benzene

Chemical Property:

• Vapor Pressure: 3.18E-07mmHg at 25°C
• Melting Point: 112 °C(Solv: ethanol (64-17-5))
• Boiling Point: 430.8°Cat760mmHg
• Flash Point: 214.3°C
• PSA: 55.05000
• Density: 1.524g/cm³
• LogP: 4.45950

Purity/Quality:

99%, ^*data from raw suppliers

1-BROMO-4-[(4-NITROBENZYL)OXY]BENZENE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-bromo-4-[(4-nitrobenzyl)oxy]benzene

There total 2 articles about 1-bromo-4-[(4-nitrobenzyl)oxy]benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.4%

4-bromo-phenol (106-41-2) + 1-bromomethyl-4-nitro-benzene (100-11-8) → (4-bromo-phenyl)-(4-nitro-benzyl)-ether (6943-02-8)

Guidance literature:

With potassium carbonate; In acetonitrile; for 7h; Reflux;

Reference yield:

4-bromo-phenol (106-41-2) + 4-nitrobenzyl chloride (100-14-1) → (4-bromo-phenyl)-(4-nitro-benzyl)-ether (6943-02-8)

Guidance literature:

With potassium carbonate; acetone;

Reference yield: 59.0%

(4-bromo-phenyl)-(4-nitro-benzyl)-ether (6943-02-8) + bis(pinacol)diborane (73183-34-3) → C19H22BNO5 (1312611-02-1)

Guidance literature:

With potassium acetate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In 1,4-dioxane; at 100 - 110 ℃; Inert atmosphere; Reflux;

upstream raw materials:

4-bromo-phenol

4-nitrobenzyl chloride

1-bromomethyl-4-nitro-benzene

Downstream raw materials:

C₁₉H₂₂BNO₅

C₂₅H₂₈N₄O₅

C₂₅H₃₀N₄O₃

C₃₅H₄₅N₅O₆

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