3-Methyl-2-pyridinecarbamic acid ethyl ester

Base Information

Chemical Name:3-Methyl-2-pyridinecarbamic acid ethyl ester
CAS No.:41322-69-4
Molecular Formula:C9H12N2O2
Molecular Weight:180.2038
Hs Code.:
DSSTox Substance ID:DTXSID50961617
Nikkaji Number:J78.912G
Wikidata:Q82943075
Mol file:41322-69-4.mol

Synonyms:3-Methyl-2-pyridinecarbamic acid ethyl ester;4-Methyl-2-pyridylurethane;41322-69-4;BRN 0475366;ethyl N-(3-methylpyridin-2-yl)carbamate;2-Pyridinecarbamic acid, 3-methyl-, ethyl ester;SCHEMBL21206911;DTXSID50961617;AKOS003854089;LS-130338;Ethyl hydrogen (3-methylpyridin-2-yl)carbonimidate

Suppliers and Price of 3-Methyl-2-pyridinecarbamic acid ethyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of 3-Methyl-2-pyridinecarbamic acid ethyl ester

Chemical Property:

Vapor Pressure:0.0307mmHg at 25°C
Boiling Point:244.2°Cat760mmHg
Flash Point:101.5°C
Density:1.163g/cm³
XLogP3:1.5
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:3
Exact Mass:180.089877630
Heavy Atom Count:13
Complexity:173

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCOC(=O)NC1=C(C=CC=N1)C

Technology Process of 3-Methyl-2-pyridinecarbamic acid ethyl ester

There total 4 articles about 3-Methyl-2-pyridinecarbamic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 64-17-5
ethanol

: N-(3-methylpyridin-2-yl)-2-naphthaleneacetamide

: 41322-69-4
(3-methyl-pyridin-2-yl)-carbamic acid ethyl ester

Guidance literature:: With copper dichloride; In dichloromethane; at 20 ℃; for 6h;

Reference yield: 35.0%

: 40927-67-1
6-methyl-[1,2]diazepine-1-carboxylic acid ethyl ester

: 41322-69-4
(3-methyl-pyridin-2-yl)-carbamic acid ethyl ester

: 75633-17-9
7-Methyl-[1,3]diazepine-1-carboxylic acid ethyl ester

Guidance literature:: In xylene; for 40h; Heating;
DOI:10.1248/cpb.29.3688

Reference yield:

: 22928-86-5
1-ethoxycarbonylimino-3-methyl-pyridinium ylide

: 41322-69-4
(3-methyl-pyridin-2-yl)-carbamic acid ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 40 percent / Irradiation

2: 50 percent / xylene / 40 h / Heating

In xylene;
DOI:10.1248/cpb.29.3688