AKOS BBS-00007799

Base Information

• Chemical Name: AKOS BBS-00007799
• CAS No.: 69517-61-9
• Molecular Formula: C12H15NO3
• Molecular Weight: 221.256
• Hs Code.: 2924299090
• Mol file: 69517-61-9.mol

Synonyms:butanoic acid,4-[(3,4-dimethylphenyl)amino]-4-oxo;Succinamic acid,N-(3,4-dimethylphenyl);3-[N-(3,4-dimethylphenyl)carbamoyl]propanoic acid;N-(3,4-Dimethyl-phenyl)-succinamidsaeure;4-[(3,4-dimethylphenyl)amino]-4-oxo-butanoic acid;N-(3,4-dimethyl-phenyl)-succinamic acid;N-(3,4-Xylyl)succinamic acid;

Chemical Property of AKOS BBS-00007799

Chemical Property:

• Vapor Pressure: 3.97E-09mmHg at 25°C
• Boiling Point: 456.5°Cat760mmHg
• Flash Point: 229.9°C
• PSA: 66.40000
• Density: 1.21g/cm³
• LogP: 2.17970

Purity/Quality:

98%min ^*data from raw suppliers

4-((3,4-Dimethylphenyl)amino)-4-oxobutanoicacid 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of AKOS BBS-00007799

There total 1 articles about AKOS BBS-00007799 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

succinic acid anhydride (108-30-5) + 4-amino-o-xylene (95-64-7) → 4-[(3,4-dimethylphenyl)amino]-4-oxo-butanoic acid (69517-61-9)

Guidance literature:

With dmap; triethylamine; In dichloromethane; at 20 ℃; for 5h;

DOI:10.1002/ardp.200800196

Reference yield: 72.0%

4-[(3,4-dimethylphenyl)amino]-4-oxo-butanoic acid (69517-61-9) → 4-[(3,4-dimethylphenyl)amino]butan-1-ol (327070-54-2)

Guidance literature:

With aluminum (III) chloride; lithium aluminium tetrahydride; In tetrahydrofuran; Reflux;

DOI:10.1002/ardp.200800196

upstream raw materials:

succinic acid anhydride

4-amino-o-xylene

Downstream raw materials:

4-[(3,4-dimethylphenyl)amino]butan-1-ol