1-{(E)-[(E)-[2-(2-chlorophenyl)hydrazinylidene](phenyl)methyl]diazenyl}-2-(4-phenylpiperazin-1-yl)ethanone

Base Information

Chemical Name:1-{(E)-[(E)-[2-(2-chlorophenyl)hydrazinylidene](phenyl)methyl]diazenyl}-2-(4-phenylpiperazin-1-yl)ethanone
CAS No.:127718-31-4
Molecular Formula:C25H25 Cl N6 O
Molecular Weight:460.9586
Hs Code.:

Synonyms:1-Piperazineaceticacid, 4-phenyl-, [[(2-chlorophenyl)azo]phenylmethylene]hydrazide (9CI)

Suppliers and Price of 1-{(E)-[(E)-[2-(2-chlorophenyl)hydrazinylidene](phenyl)methyl]diazenyl}-2-(4-phenylpiperazin-1-yl)ethanone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemicals and raw materials
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Total 1 raw suppliers

Chemical Property of 1-{(E)-[(E)-[2-(2-chlorophenyl)hydrazinylidene](phenyl)methyl]diazenyl}-2-(4-phenylpiperazin-1-yl)ethanone

Chemical Property:

Vapor Pressure:0mmHg at 25°C
Boiling Point:598°Cat760mmHg
Flash Point:315.5°C
Density:1.25g/cm³

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1-{(E)-[(E)-[2-(2-chlorophenyl)hydrazinylidene](phenyl)methyl]diazenyl}-2-(4-phenylpiperazin-1-yl)ethanone

There total 3 articles about 1-{(E)-[(E)-[2-(2-chlorophenyl)hydrazinylidene](phenyl)methyl]diazenyl}-2-(4-phenylpiperazin-1-yl)ethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 100-52-7
benzaldehyde

: 127718-31-4
(4-Phenyl-piperazin-1-yl)-acetic acid [1-(2-chloro-phenylazo)-1-phenyl-meth-(E)-ylidene]-hydrazide

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / acetic acid / ethanol / 5 h / Heating

2: 1.) sodium nitrite, HCl / 1.) gl. acetic acid, 0-5 deg C, 2.) pyridine, RT, overnight

With hydrogenchloride; acetic acid; sodium nitrite; In ethanol;

Reference yield:

: 1689-05-0
4-phenyl-1-piperazineacetic acid hydrazide

: 127718-31-4
(4-Phenyl-piperazin-1-yl)-acetic acid [1-(2-chloro-phenylazo)-1-phenyl-meth-(E)-ylidene]-hydrazide

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / acetic acid / ethanol / 5 h / Heating

2: 1.) sodium nitrite, HCl / 1.) gl. acetic acid, 0-5 deg C, 2.) pyridine, RT, overnight

With hydrogenchloride; acetic acid; sodium nitrite; In ethanol;

Reference yield:

: 95-51-2
o-chloroaniline

: 67041-03-6
4-phenyl-1-piperazineacetic acid benzylidenehydrazide

: 127718-31-4
(4-Phenyl-piperazin-1-yl)-acetic acid [1-(2-chloro-phenylazo)-1-phenyl-meth-(E)-ylidene]-hydrazide

Guidance literature:: With hydrogenchloride; sodium nitrite; Yield given. Multistep reaction; 1.) gl. acetic acid, 0-5 deg C, 2.) pyridine, RT, overnight;