N-(4-fluorophenyl)-2-[(E)-(6-oxocyclohexa-2,4-dien-1-ylidene)methyl]hydrazinecarbothioamide

Base Information

Chemical Name:N-(4-fluorophenyl)-2-[(E)-(6-oxocyclohexa-2,4-dien-1-ylidene)methyl]hydrazinecarbothioamide
CAS No.:16113-37-4
Molecular Formula:C14H12 F N3 O S
Molecular Weight:289.333
Hs Code.:
Mol file:16113-37-4.mol

Synonyms:Semicarbazide,4-(p-fluorophenyl)-1-salicylidene-3-thio- (8CI); NSC 73241

Suppliers and Price of N-(4-fluorophenyl)-2-[(E)-(6-oxocyclohexa-2,4-dien-1-ylidene)methyl]hydrazinecarbothioamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of N-(4-fluorophenyl)-2-[(E)-(6-oxocyclohexa-2,4-dien-1-ylidene)methyl]hydrazinecarbothioamide

Chemical Property:

Vapor Pressure:3.22E-07mmHg at 25°C
Boiling Point:418.7°Cat760mmHg
Flash Point:207°C
Density:1.465g/cm³

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of N-(4-fluorophenyl)-2-[(E)-(6-oxocyclohexa-2,4-dien-1-ylidene)methyl]hydrazinecarbothioamide

There total 2 articles about N-(4-fluorophenyl)-2-[(E)-(6-oxocyclohexa-2,4-dien-1-ylidene)methyl]hydrazinecarbothioamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 330-94-9
4-(4-fluorophenyl)thiosemicarbazide

: 90-02-8
salicylaldehyde

: 16113-37-4
4-(4-fluorophenyl)-1-[(2-hydroxyphenyl)methylidene]-3-thiosemicarbazide

Guidance literature:: In methanol;
DOI:10.1016/j.poly.2012.11.031

Reference yield:

: 371-40-4
4-fluoroaniline

: 16113-37-4
4-(4-fluorophenyl)-1-[(2-hydroxyphenyl)methylidene]-3-thiosemicarbazide

Guidance literature:: Multi-step reaction with 2 steps

1: (i) aq. NH₃, (ii) N₂H₄*H₂O, ClCH₂CO₂Na

2: AcOH / ethanol / Heating

With acetic acid; In ethanol;