2,4-DICHLORO-1-(2-PROPYNYLOXY)BENZENE

Base Information

• Chemical Name: 2,4-DICHLORO-1-(2-PROPYNYLOXY)BENZENE
• CAS No.: 17061-90-4
• Molecular Formula: C9H6Cl2O
• Molecular Weight: 201.052
• Hs Code.: 2909309090
• Mol file: 17061-90-4.mol

Synonyms:Benzene,2,4-dichloro-1-(2-propynyloxy)- (9CI);Ether, 2,4-dichlorophenyl 2-propynyl(8CI);2,4-Dichloro-1-(prop-2-ynyloxy)benzene;2,4-Dichlorophenyl 2-propynylether;2,4-Dichlorophenyl propargyl ether;3-(2,4-Dichlorophenoxy)-1-propyne;3-(2,4-Dichlorophenoxy)propyne;

Chemical Property of 2,4-DICHLORO-1-(2-PROPYNYLOXY)BENZENE

Chemical Property:

• Vapor Pressure: 0.00853mmHg at 25°C
• Melting Point: 47-49 °C
• Refractive Index: 1.559
• Boiling Point: 275.5 °C at 760 mmHg
• Flash Point: 117.6 °C
• PSA: 9.23000
• Density: 1.304g/cm³
• LogP: 3.00540
• Storage Temp.: 2-8°C

Purity/Quality:

97% ^*data from raw suppliers

2,4-Dichloro-1-(2-propynyloxy)benzene ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xi
• Hazard Codes: Xi
• Statements: 36/37/38-41
• Safety Statements: 26-36/37/39-39

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2,4-DICHLORO-1-(2-PROPYNYLOXY)BENZENE

There total 7 articles about 2,4-DICHLORO-1-(2-PROPYNYLOXY)BENZENE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

propargyl bromide (106-96-7) + 2,4-dichlorophenol (120-83-2,40477-79-0) → 2,4-dichloro-1-(prop-2-yn-1-yloxy)benzene (17061-90-4)

Guidance literature:

With potassium carbonate; In tetrahydrofuran;

DOI:10.1016/j.tetlet.2008.04.150

Reference yield: 66.0%

1-chloro-4-(prop-2-yn-1-yloxy)benzene (19130-39-3) → 2,4-dichloro-1-(prop-2-yn-1-yloxy)benzene (17061-90-4)

Guidance literature:

With chlorine; copper(l) chloride; In tetrachloromethane; at 70 ℃;

Reference yield:

→ 2,4-dichloro-1-(prop-2-yn-1-yloxy)benzene (17061-90-4)

Guidance literature:

With potassium hydroxide;

DOI:10.1021/ja01354a034

upstream raw materials:

1-chloro-4-(prop-2-yn-1-yloxy)benzene

propargyl bromide

2,4-dichlorophenol

(2,3-dibromo-propyl)-(2,4-dichloro-phenyl)-ether

Downstream raw materials:

2,4-dichloro-1-[(3-iodoprop-2-yn-1-yl)oxy]benzene