2,4-Dichloro-6-(4-chlorophenoxy)-1,3,5-triazine

Base Information

• Chemical Name: 2,4-Dichloro-6-(4-chlorophenoxy)-1,3,5-triazine
• CAS No.: 30886-26-1
• Molecular Formula: C9H4 Cl3 N3 O
• Molecular Weight: 276.509
• DSSTox Substance ID: DTXSID50275347
• Nikkaji Number: J1.615.400H
• Wikidata: Q82005125
• Mol file: 30886-26-1.mol

Synonyms:2,4-dichloro-6-(4-chlorophenoxy)-1,3,5-triazine;30886-26-1;SCHEMBL17563555;DTXSID50275347;AKOS009154263;FT-0708579;2,4-DICHLORO-6-(P-CHLOROPHENOXY)-S-TRIAZINE

Chemical Property of 2,4-Dichloro-6-(4-chlorophenoxy)-1,3,5-triazine

Chemical Property:

• Vapor Pressure: 5.7E-08mmHg at 25°C
• Melting Point: 111 °C
• Boiling Point: 453.1°Cat760mmHg
• Flash Point: 227.8°C
• PSA: 47.90000
• Density: 1.575g/cm³
• LogP: 3.62410
• XLogP3: 4.4
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 2
• Exact Mass: 274.941995
• Heavy Atom Count: 16
• Complexity: 216

Purity/Quality:

99% ^*data from raw suppliers

2,4-DICHLORO-6-(4-CHLOROPHENOXY)-1,3,5-TRIAZINE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC(=CC=C1OC2=NC(=NC(=N2)Cl)Cl)Cl

Technology Process of 2,4-Dichloro-6-(4-chlorophenoxy)-1,3,5-triazine

There total 2 articles about 2,4-Dichloro-6-(4-chlorophenoxy)-1,3,5-triazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

1,3,5-trichloro-2,4,6-triazine (108-77-0) + 4-chloro-phenol (106-48-9,82344-39-6) → 2,4-dichloro-6-(4-chlorophenoxy)-1,3,5-triazine (30886-26-1)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; at -35 - 20 ℃; for 30h;

DOI:10.1007/s00706-018-2212-0

Reference yield:

→ 2,4-dichloro-6-(4-chlorophenoxy)-1,3,5-triazine (30886-26-1)

Guidance literature:

/BRN= 135423/;

Reference yield:

2,4-dichloro-6-(4-chlorophenoxy)-1,3,5-triazine (30886-26-1) + 4-hydroxy-benzaldehyde (123-08-0,65581-83-1) → 4-(4-chloro-6-(4-chlorophenoxy)-1,3,5-triazin-2-yloxy)benzaldehyde

Guidance literature:

With triethylamine; In dichloromethane; at 0 - 20 ℃; for 2h;

DOI:10.1016/j.tet.2014.12.072

upstream raw materials:

1,3,5-trichloro-2,4,6-triazine

4-chloro-phenol

Downstream raw materials:

2,4-diphenoxy-6-chloro-s-triazine

2-chloro-4,6-bis-(4-chloro-phenoxy)-[1,3,5]triazine

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