1-Methyl-2-[(5-nitrofuran-2-yl)methylidene]hydrazine

Base Information

• Chemical Name: 1-Methyl-2-[(5-nitrofuran-2-yl)methylidene]hydrazine
• CAS No.: 7511-57-1
• Molecular Formula: C6H7N3O3
• Molecular Weight: 169.1381
• DSSTox Substance ID: DTXSID00996611

Synonyms:7511-57-1;1-methyl-2-[(5-nitrofuran-2-yl)methylidene]hydrazine;DTXSID00996611

Chemical Property of 1-Methyl-2-[(5-nitrofuran-2-yl)methylidene]hydrazine

Chemical Property:

• Vapor Pressure: 0.00162mmHg at 25°C
• Boiling Point: 294.5°Cat760mmHg
• Flash Point: 131.9°C
• Density: 1.39g/cm³
• XLogP3: 0.6
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 5
• Rotatable Bond Count: 2
• Exact Mass: 169.04874109
• Heavy Atom Count: 12
• Complexity: 189

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CNN=CC1=CC=C(O1)[N+](=O)[O-]

Technology Process of 1-Methyl-2-[(5-nitrofuran-2-yl)methylidene]hydrazine

There total 2 articles about 1-Methyl-2-[(5-nitrofuran-2-yl)methylidene]hydrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

5-nitrofurane-2-carboxaldehyde (698-63-5) + methylhydrazine sulfuric acid (302-15-8) → 5-nitro-2-furancarboxaldehyde methylhydrazone (7511-57-1)

Guidance literature:

With sodium hydroxide; In methanol; water; at 20 ℃; Darkness;

DOI:10.1021/acs.chemrestox.8b00362

Reference yield:

→ 5-nitro-2-furancarboxaldehyde methylhydrazone (7511-57-1)

Guidance literature:

5-Nitro-furfural, Methyl-hydrazin/absol. A.;

DOI:10.1021/jo01038a514

Reference yield: 91.0%

5-nitro-2-furancarboxaldehyde methylhydrazone (7511-57-1) + (E)-3-benzylidenechroman-4-one (30779-90-9) → 2',4'-dihydro-2'-methyl-5'-(5-nitro-2-furanyl)-4'-phenyl[spiro[2H]-1-benzopyran-3(4H),3'-[3H]pyrazol]-4-one

Guidance literature:

With chloroamine-T; In methanol; Heating;

DOI:10.1002/jhet.5570360442

upstream raw materials:

5-nitrofurane-2-carboxaldehyde

methylhydrazine sulfuric acid

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