2-CHLORO-6-NITROBENZAMIDE

Base Information

• Chemical Name: 2-CHLORO-6-NITROBENZAMIDE
• CAS No.: 107485-64-3
• Molecular Formula: C7H5 Cl N2 O3
• Molecular Weight: 200.581
• Hs Code.: 2924299090
• Mol file: 107485-64-3.mol

Synonyms:2-Chloro-6-nitrobenzamide

Chemical Property of 2-CHLORO-6-NITROBENZAMIDE

Chemical Property:

• Vapor Pressure: 0.00171mmHg at 25°C
• Melting Point: 185°C
• Boiling Point: 293.6°C at 760 mmHg
• Flash Point: 131.4°C
• PSA: 88.91000
• Density: 1.52g/cm³
• LogP: 2.57060

Purity/Quality:

99% ^*data from raw suppliers

2-Chloro-6-nitrobenzamide ^*data from reagent suppliers

Safty Information:

• Pictogram(s): R36/37/38:Irritating to eyes, respiratory system and skin.
• Hazard Codes: R36/37/38:Irritating to eyes, respiratory system and skin.
• Statements: 36/37/38
• Safety Statements: 26-36

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-CHLORO-6-NITROBENZAMIDE

There total 1 articles about 2-CHLORO-6-NITROBENZAMIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ 2-chloro-6-nitro-benzoic acid amide (107485-64-3)

Guidance literature:

With ammonium hydroxide;

DOI:10.1002/hlca.19440270175

Reference yield: 85.0%

2-chloro-6-nitro-benzoic acid amide (107485-64-3) + benzyl alcohol (100-51-6,185532-71-2) → 5-chloro-2-phenylquinazolin-4(3H)-one (19407-57-9)

Guidance literature:

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In chlorobenzene; at 140 ℃; for 8h; Inert atmosphere; Sealed tube;

DOI:10.1039/d1ra01755a

Reference yield: 72.0%

2-chloro-6-nitro-benzoic acid amide (107485-64-3) + diphenyldisulfane (882-33-7) → 2-chloro-6-nitro-N-(phenylthio)benzamide

Guidance literature:

2-chloro-6-nitro-benzoic acid amide; With sodium hydride; In tetrahydrofuran; mineral oil; at 20 ℃; for 1h;

diphenyldisulfane; In tetrahydrofuran; mineral oil; at 20 ℃; for 36h;

DOI:10.1080/10426507.2015.1012670

Downstream raw materials:

2-chloro-N-(2-chloro-3-fluoropyridin-4-yl)-6-nitrobenzamide

2-chloro-N-(2-((2-(4,5-dihydrooxazol-2-yl)phenyl)carbamoyl)phenyl)-6-nitrobenzamide

5-chloro-2-phenylquinazolin-4(3H)-one