3-hydroxy-4,4,4-trichlorobutyric beta-lactone

Base Information Edit

Chemical Name:3-hydroxy-4,4,4-trichlorobutyric beta-lactone
CAS No.:5895-35-2
Molecular Formula:C4H3Cl3O2
Molecular Weight:189.4244
Hs Code.:
Mol file:5895-35-2.mol

Synonyms:2-oxetanone, 4-(trichloromethyl)-;3-Hydroxy-4,4,4-trichlorobutyric b-lactone;4-(Trichloromethyl)oxetan-2-one;

Suppliers and Price of 3-hydroxy-4,4,4-trichlorobutyric beta-lactone

Supply Marketing:Edit

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
3-HYDROXY-4,4,4-TRICHLOROBUTYRIC BETA-LACTONE 95.00%
5MG
$ 501.08

Total 8 raw suppliers

Chemical Property of 3-hydroxy-4,4,4-trichlorobutyric beta-lactone Edit

Chemical Property:

Vapor Pressure:0.075mmHg at 25°C
Refractive Index:1.541
Boiling Point:228 °C at 760 mmHg
Flash Point:104 °C
PSA：26.30000
Density:1.731 g/cm³
LogP:1.67210

Purity/Quality:

99% ^*data from raw suppliers

3-HYDROXY-4,4,4-TRICHLOROBUTYRIC BETA-LACTONE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 3-hydroxy-4,4,4-trichlorobutyric beta-lactone

There total 2 articles about 3-hydroxy-4,4,4-trichlorobutyric beta-lactone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 75-87-6
chloral

: 75-36-5
acetyl chloride

: 5895-35-2,16493-62-2,20710-33-2
4-trichloromethyloxetan-2-one

Guidance literature:: With triethylamine; In diethyl ether; at 0 - 20 ℃; for 2.5h; Inert atmosphere;
DOI:10.1055/s-0036-1588169

Reference yield:

: 5895-35-2,16493-62-2,20710-33-2
4-trichloromethyloxetan-2-one

Guidance literature:: 1.) Eintropf. einer Lsg. v. (C2H5)3N in Ae. in eine Lsg. v. Chloral + Acetylchlorid in Ae. (0-10grad; 1/2 Std.), 2.) Befr. v. ausgefallenen (C2H5)3N, HCl;