Technology Process of Tungsten chloride (WCl3)
There total 9 articles about Tungsten chloride (WCl3) which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
In
neat (no solvent);
mixt. of educts held at 300-350°C for 2-3 h; WOCl4 sepd. by sublimation at 250°C; the residue held at 450-470°C for 3-4 h; WOCl4 sepd. once more by sublimation at 350-370°C; cooled; elem.anal., XRD;
- Guidance literature:
-
In
neat (no solvent);
mixt. of educts held at 300-350°C for 2-3 h; WOCl4 sepd. by sublimation at 250°C; the residue held at 450-470°C for 3-4 h; WOCl4 sepd. once more by sublimation at 350-370°C; cooled; elem.anal., XRD;
- Guidance literature:
-
In
neat (no solvent);
byproducts: O2; reaction in flow of Ar and Cl2, at temperature range 50-950°C;
Kinetics;
DOI:10.1016/j.tca.2012.02.015
