2-Phenylphthalazin-1(2h)-one

Base Information

Chemical Name:2-Phenylphthalazin-1(2h)-one
CAS No.:6266-49-5
Molecular Formula:C14H10N2O
Molecular Weight:222.246
Hs Code.:
NSC Number:37228
DSSTox Substance ID:DTXSID50284439
Nikkaji Number:J832.759I
Wikidata:Q82019390

Synonyms:2-phenylphthalazin-1(2h)-one;6266-49-5;2-phenyl-1-phthalazinone;2-phenyl-1,2-dihydrophthalazin-1-one;2-phenyl-1(2H)-phthalazinone;2-phenylphthalazin-1-one;NSC37228;Maybridge1_003252;SCHEMBL4238032;HMS550L18;DTXSID50284439;BCCBXCGRKOKWBZ-UHFFFAOYSA-N;MFCD00278209;NSC-37228;STK661465;AKOS002275110;CCG-124570;CS-16241;CS-0094241;D72122

Suppliers and Price of 2-Phenylphthalazin-1(2h)-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 9 raw suppliers

Chemical Property of 2-Phenylphthalazin-1(2h)-one

Chemical Property:

Vapor Pressure:2.53E-06mmHg at 25°C
Boiling Point:391.1°Cat760mmHg
Flash Point:190.3°C
Density:1.19g/cm³
XLogP3:2.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:222.079312947
Heavy Atom Count:17
Complexity:320

Purity/Quality:: NLT 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)N2C(=O)C3=CC=CC=C3C=N2

Technology Process of 2-Phenylphthalazin-1(2h)-one

There total 26 articles about 2-Phenylphthalazin-1(2h)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 100-63-0
phenylhydrazine

: 119-67-5
o-carboxybenzaldehyde

: 6266-49-5
2-phenylphthalazin-1-one

Guidance literature:: With hydrogen; platinum; In 1,4-dioxane; at 80 ℃; for 0.5h; under 750.075 Torr; Sealed tube;
DOI:10.1021/ol300471a

Reference yield: 85.5%

: 15226-74-1,61091-28-9,61117-58-6
dicobalt octacarbonyl

: 59-88-1
phenylhydrazine hydrochloride

: 6630-33-7
ortho-bromobenzaldehyde

: 6266-49-5
2-phenylphthalazin-1-one

Guidance literature:: With 1,1'-bis-(diphenylphosphino)ferrocene; palladium diacetate; 1,8-diazabicyclo[5.4.0]undec-7-ene; In N,N-dimethyl-formamide; at 90 ℃; for 3h; Sealed tube; Molecular sieve;
DOI:10.1016/j.tetlet.2014.04.082

Reference yield: 85.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 610-94-6
2-bromobenzoic acid methyl ester

: 100-63-0
phenylhydrazine

: 6266-49-5
2-phenylphthalazin-1-one

Guidance literature:: With palladium(II) trifluoroacetate; potassium carbonate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; In toluene; at 150 ℃; for 24h; Reagent/catalyst; Temperature; Solvent; Catalytic behavior;
DOI:10.1021/ol502498y