N,N-Diethyl-3-hydroxy-4,4,4-trichlorobutyramide

Base Information

Chemical Name:N,N-Diethyl-3-hydroxy-4,4,4-trichlorobutyramide
CAS No.:25290-15-7
Molecular Formula:C₈H₁₄Cl₃NO₂
Molecular Weight:262.564
Hs Code.:
DSSTox Substance ID:DTXSID00948130
Nikkaji Number:J65.822G

Synonyms:BRN 1949650;N,N-Diethyl-3-hydroxy-4,4,4-trichlorobutyramide;(N,N-Diethylaminocarbonyl)methyl trichloromethyl carbinol;25290-15-7;BUTYRAMIDE, N,N-DIETHYL-3-HYDROXY-4,4,4-TRICHLORO-;4,4,4-trichloro-N,N-diethyl-3-hydroxybutanamide;C8H14Cl3NO2;C8-H14-Cl3-N-O2;DTXSID00948130;LS-47630

Suppliers and Price of N,N-Diethyl-3-hydroxy-4,4,4-trichlorobutyramide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 0 raw suppliers

Chemical Property of N,N-Diethyl-3-hydroxy-4,4,4-trichlorobutyramide

Chemical Property:

Vapor Pressure:9.65E-06mmHg at 25°C
Boiling Point:333.5°Cat760mmHg
Flash Point:155.5°C
Density:1.332g/cm³
XLogP3:1.6
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:4
Exact Mass:261.009012
Heavy Atom Count:14
Complexity:190

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCN(CC)C(=O)CC(C(Cl)(Cl)Cl)O

Technology Process of N,N-Diethyl-3-hydroxy-4,4,4-trichlorobutyramide

There total 5 articles about N,N-Diethyl-3-hydroxy-4,4,4-trichlorobutyramide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2315-36-8
2-Chloro-N,N-diethylacetamide

: 25290-15-7
4,4,4-Trichloro-N,N-diethyl-3-hydroxy-butyramide

Guidance literature:: Multi-step reaction with 3 steps

1: 75 percent / lithium / tetrahydrofuran / 15 h / Ambient temperature

2: 83 percent / 2 h / 90 - 100 °C

3: methanol / 3 h / Heating

With lithium; In tetrahydrofuran; methanol;