4,6-Dimethyl-2-oxo-1-[(phenylmethylidene)amino]-1,2-dihydropyridine-3-carbonitrile

Base Information

Chemical Name:4,6-Dimethyl-2-oxo-1-[(phenylmethylidene)amino]-1,2-dihydropyridine-3-carbonitrile
CAS No.:89814-99-3
Molecular Formula:C₁₅H₁₃N₃O
Molecular Weight:251.288
Hs Code.:
European Community (EC) Number:654-397-6
NSC Number:108199
ChEMBL ID:CHEMBL3193539

Synonyms:MLS000055041;SMR000065848;4,6-dimethyl-2-oxo-1-[(phenylmethylidene)amino]-1,2-dihydropyridine-3-carbonitrile;89814-99-3;NSC108199;1-(benzylideneamino)-4,6-dimethyl-2-oxopyridine-3-carbonitrile;cid_268105;CHEMBL3193539;BDBM45347;STK013076;AKOS000487495;NSC-108199;SR-01000082089;SR-01000082089-1;1-(benzalamino)-2-keto-4,6-dimethyl-nicotinonitrile;Z56788816;4,6-dimethyl-2-oxo-1-[(phenylmethylene)amino]-3-pyridinecarbonitrile;4,6-dimethyl-2-oxidanylidene-1-[(phenylmethylidene)amino]pyridine-3-carbonitrile;4,6-dimethyl-2-oxo-1-{[(1E)-phenylmethylene]amino}-1,2-dihydropyridine-3-carbonitrile;4,6-dimethyl-2-oxo-1-{[(E)-phenylmethylidene]amino}-1,2-dihydropyridine-3-carbonitrile;4,6-DIMETHYL-2-OXO-1-[(E)-(PHENYLMETHYLIDENE)AMINO]-1,2-DIHYDROPYRIDINE-3-CARBONITRILE

Suppliers and Price of 4,6-Dimethyl-2-oxo-1-[(phenylmethylidene)amino]-1,2-dihydropyridine-3-carbonitrile

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of 4,6-Dimethyl-2-oxo-1-[(phenylmethylidene)amino]-1,2-dihydropyridine-3-carbonitrile

Chemical Property:

Vapor Pressure:3.37E-06mmHg at 25°C
Boiling Point:387.1°Cat760mmHg
Flash Point:187.9°C
Density:1.11g/cm³
XLogP3:2.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:2
Exact Mass:251.105862047
Heavy Atom Count:19
Complexity:513

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC(=C(C(=O)N1N=CC2=CC=CC=C2)C#N)C
Isomeric SMILES:CC1=CC(=C(C(=O)N1/N=C/C2=CC=CC=C2)C#N)C

Technology Process of 4,6-Dimethyl-2-oxo-1-[(phenylmethylidene)amino]-1,2-dihydropyridine-3-carbonitrile

There total 4 articles about 4,6-Dimethyl-2-oxo-1-[(phenylmethylidene)amino]-1,2-dihydropyridine-3-carbonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 4974-44-1,180793-11-7
N'-benzylidene-2-cyanoacetohydrazide

: 123-54-6,81235-32-7
acetylacetone

: 89814-99-3
1-benzalimino-4,6-diamino-2(2H)-pyridinone-3-carbonitrile

Guidance literature:: In N,N-dimethyl-formamide; for 2h; Heating;

Reference yield:

: 100-52-7
benzaldehyde

: 89814-99-3
1-benzalimino-4,6-diamino-2(2H)-pyridinone-3-carbonitrile

Guidance literature:: Multi-step reaction with 2 steps

1: 78 percent / 0.33 h / Heating

2: 65 percent / triethylamine / ethanol / 7 h / Heating

With triethylamine; In ethanol;
DOI:10.1002/ardp.19843170303

Reference yield:

: 100-52-7
benzaldehyde

: 89814-99-3
1-benzalimino-4,6-diamino-2(2H)-pyridinone-3-carbonitrile

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / piperidine / ethanol / 2 h / Heating

2: 75 percent / dimethylformamide / 2 h / Heating

With piperidine; In ethanol; N,N-dimethyl-formamide;