Triethoxyfluorosilane

Base Information

• Chemical Name: Triethoxyfluorosilane
• CAS No.: 358-60-1
• Molecular Formula: C6H15FO3Si
• Molecular Weight: 182.267
• Hs Code.: 29319090
• European Community (EC) Number: 671-367-8
• DSSTox Substance ID: DTXSID0075233
• Nikkaji Number: J707.466B
• Wikidata: Q72477183
• Mol file: 358-60-1.mol

Synonyms:TEFS cpd;triethoxyfluorosilane

Chemical Property of Triethoxyfluorosilane

Chemical Property:

• Melting Point: 134-135 °C
• Refractive Index: 1.36
• Boiling Point: 132.4 °C at 760 mmHg
• Flash Point: 33.9 °C
• PSA: 27.69000
• Density: 0.97 g/cm³
• LogP: 1.50100
• Sensitive.: Moisture Sensitive
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 6
• Exact Mass: 182.07744903
• Heavy Atom Count: 11
• Complexity: 84.8

Purity/Quality:

97% ^*data from raw suppliers

Triethoxyfluorosilane ^*data from reagent suppliers

Safty Information:

• Pictogram(s): C
• Hazard Codes: C
• Statements: 34
• Safety Statements: 26-36/37/39-45

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCO[Si](OCC)(OCC)F

Technology Process of Triethoxyfluorosilane

There total 13 articles about Triethoxyfluorosilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(pentafluoro phenyl) triethoxy silane (20083-34-5) → triethoxyfluorosilane (358-60-1) + Pentafluorobenzene (363-72-4) + trifluoro(pentafluorophenyl)silane (5272-26-4)

Guidance literature:

With hydrogen fluoride; In ethanol; at -40 ℃; for 1h; Yield given. Yields of byproduct given;

DOI:10.1016/0022-328X(95)05676-G

Reference yield:

chlorotriethoxysilane (4667-99-6) → triethoxyfluorosilane (358-60-1)

Guidance literature:

With antimony(III) fluoride;

DOI:10.1038/158672b0

Reference yield:

tetraethoxy orthosilicate (78-10-4) + antimony(III) fluoride (7783-56-4) → triethoxyfluorosilane (358-60-1)

Guidance literature:

With antimonypentachloride; heating;;

DOI:10.1038/158672b0

upstream raw materials:

tetraethoxy orthosilicate

difluorodiethoxysilane

chlorotriethoxysilane

(pentafluoro phenyl) triethoxy silane

Downstream raw materials:

difluorodiethoxysilane

diethyl phenylboronate

(-)S β-hydroxy β-phenyl n-butanoate de methyle

(R)-3-hydroxy-3-phenylbutyric acid methyl ester