1,3-Dimethyl-5-[(2-methylprop-2-en-1-yl)oxy]benzene

Base Information

Chemical Name:1,3-Dimethyl-5-[(2-methylprop-2-en-1-yl)oxy]benzene
CAS No.:3698-47-3
Molecular Formula:C12H16O
Molecular Weight:176.258
Hs Code.:
NSC Number:86598
DSSTox Substance ID:DTXSID80958151
Wikidata:Q82938654

Synonyms:3698-47-3;1,3-dimethyl-5-[(2-methylprop-2-en-1-yl)oxy]benzene;NSC86598;NCIOpen2_001147;DTXSID80958151;NSC-86598;AKOS008949169

Suppliers and Price of 1,3-Dimethyl-5-[(2-methylprop-2-en-1-yl)oxy]benzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of 1,3-Dimethyl-5-[(2-methylprop-2-en-1-yl)oxy]benzene

Chemical Property:

Vapor Pressure:0.0164mmHg at 25°C
Boiling Point:263.9°C at 760 mmHg
Flash Point:100.3°C
Density:0.925g/cm³
XLogP3:3.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:3
Exact Mass:176.120115130
Heavy Atom Count:13
Complexity:164

Purity/Quality:: 95% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC(=CC(=C1)OCC(=C)C)C

Technology Process of 1,3-Dimethyl-5-[(2-methylprop-2-en-1-yl)oxy]benzene

There total 3 articles about 1,3-Dimethyl-5-[(2-methylprop-2-en-1-yl)oxy]benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 108-68-9,50356-23-5
3,5-Dimethylphenol

: 563-47-3
3-Chloro-2-methylpropene

: 3698-47-3
1,3-dimethyl-5-(2-methylallyloxy)benzene

Guidance literature:: With potassium carbonate; potassium iodide; In N,N-dimethyl-formamide; acetone; Heating;

Reference yield: 62.0%

: 18621-26-6
1-(3,5-dimethylphenoxy)-2-propanone

: 1779-49-3
Methyltriphenylphosphonium bromide

: 3698-47-3
1,3-dimethyl-5-(2-methylallyloxy)benzene

Guidance literature:: With potassium tert-butylate; In tetrahydrofuran; at 0 ℃; for 2h; Inert atmosphere;
DOI:10.1039/d1cc05684k

Reference yield: 45.0%

: 820-71-3
methallyl acetate

: 108-68-9,50356-23-5
3,5-Dimethylphenol

: 3698-47-3
1,3-dimethyl-5-(2-methylallyloxy)benzene

Guidance literature:: With [Ru(PPh₃)₂(2,2’-bipyridine)(MeCN)Cl][BPh₄]; potassium carbonate; In toluene; for 15h; regioselective reaction; Schlenk technique; Reflux;
DOI:10.1016/j.jorganchem.2014.08.014