Dodecyl isocyanide

Base Information

• Chemical Name: Dodecyl isocyanide
• CAS No.: 36999-98-1
• Molecular Formula: C13H26N+
• Molecular Weight: 195.348
• Hs Code.: 2926909090
• Mol file: 36999-98-1.mol

Synonyms:n-dodecyl isocyanide;dodecane-1-isonitrile;Dodecylisocyanid;1-dodecaneisonitrile;n-Dodecyl-isonitril;dodecyl isocyanide;n-dodecyl isonitrile;

Chemical Property of Dodecyl isocyanide

Chemical Property:

• Boiling Point: °Cat760mmHg
• Flash Point: °C
• PSA: 0.00000
• Density: g/cm³
• LogP: 4.05730

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Dodecyl isocyanide

There total 7 articles about Dodecyl isocyanide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

N-1-dodecylformamide (7402-57-5) → dodecane-1-isonitrile (36999-98-1)

Guidance literature:

With pyridine; p-toluenesulfonyl chloride; at 20 ℃; for 24h; Cooling; Green chemistry;

DOI:10.1039/c9gc04070f

Reference yield:

n-Dodecylamine (124-22-1) + chloroform (67-66-3,8013-54-5) → dodecane-1-isonitrile (36999-98-1)

Guidance literature:

With potassium hydroxide; butan-1-ol;

Reference yield:

n-Dodecylamine (124-22-1) → dodecane-1-isonitrile (36999-98-1)

Guidance literature:

Multi-step reaction with 2 steps

1: 92 percent / 3 h / Heating

2: 54 percent / Et₃N; phosphoryl chloride / CH₂Cl₂ / 2 h / 0 - 20 °C

With triethylamine; trichlorophosphate; In dichloromethane;

DOI:10.1021/ol034073+

upstream raw materials:

n-Dodecylamine

chloroform

N-1-dodecylformamide

n-Octylamine

Downstream raw materials:

C₆₂H₈₂N₂O₁₂