2,2-DIMETHYL-BENZO[1,3]DIOXOL-5-YLAMINE

Base Information

• Chemical Name: 2,2-DIMETHYL-BENZO[1,3]DIOXOL-5-YLAMINE
• CAS No.: 6324-89-6
• Molecular Formula: C₉H₁₁NO₂
• Molecular Weight: 165.192
• Hs Code.: 2932999099
• Mol file: 6324-89-6.mol

Synonyms:(2,2-Dimethylbenzodioxol-5-yl)amine;3,4-Isopropylidenedioxyaniline; 5-Amino-2,2-dimethyl-1,3-benzodioxole; NSC31736

Chemical Property of 2,2-DIMETHYL-BENZO[1,3]DIOXOL-5-YLAMINE

Chemical Property:

• Vapor Pressure: 0.00732mmHg at 25°C
• Melting Point: 170.5-172℃
• Refractive Index: 1.5520 (20℃)
• Boiling Point: 138-144℃ (12 Torr)
• Flash Point: 126.3°C
• PSA: 44.48000
• Density: 1.169g/cm³
• LogP: 2.35730

Purity/Quality:

99%, ^*data from raw suppliers

2,2-Dimethyl-2H-1,3-benzodioxol-5-amine ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2,2-DIMETHYL-BENZO[1,3]DIOXOL-5-YLAMINE

There total 5 articles about 2,2-DIMETHYL-BENZO[1,3]DIOXOL-5-YLAMINE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,2-dimethyl-5-nitro-1,3-benzodioxole (54186-68-4) → 2,2-dimethylbenzo[d][1,3]dioxol-5-ylamine (6324-89-6)

Guidance literature:

With 1,4-dioxane; palladium on activated charcoal; at 60 - 90 ℃; under 73550.8 Torr; Hydrogenation;

DOI:10.1002/hlca.19530360323

Reference yield:

2,2-dimethyl-1,3-benzodioxole (14005-14-2) → 2,2-dimethylbenzo[d][1,3]dioxol-5-ylamine (6324-89-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 95 percent / 60percent nitric acid / 1 h / 50 °C

2: H₂ / Adams catalyst / ethanol / 1 h

With hydrogen; nitric acid; platinum(IV) oxide; In ethanol;

Reference yield:

benzene-1,2-diol (120-80-9,19481-10-8,37349-32-9) → 2,2-dimethylbenzo[d][1,3]dioxol-5-ylamine (6324-89-6)

Guidance literature:

Multi-step reaction with 3 steps

1: 70 percent / p-toluenesulfonic acid / benzene / 48 h / Heating

2: 95 percent / 60percent nitric acid / 1 h / 50 °C

3: H₂ / Adams catalyst / ethanol / 1 h

With hydrogen; nitric acid; toluene-4-sulfonic acid; platinum(IV) oxide; In ethanol; benzene;

upstream raw materials:

2,2-dimethyl-5-nitro-1,3-benzodioxole

2,2-dimethyl-1,3-benzodioxole

benzene-1,2-diol

Downstream raw materials:

N-(2,2-dimethylbenzo[1,3]dioxol-5-yl)acetamide

N²-cyclohexyl-3-nitro-2-aminopyridine

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 6324-89-6 2,2-DIMETHYL-BENZO[1,3]DIOXOL-5-YLAMINE

Send

Send

Metric Ton KG G Pound L ML

Send

Send