S-[2-(diethylamino)ethyl] benzenecarbothioate

Base Information

• Chemical Name: S-[2-(diethylamino)ethyl] benzenecarbothioate
• CAS No.: 14441-55-5
• Molecular Formula: C13H19 N O S
• Molecular Weight: 237.366
• Mol file: 14441-55-5.mol

Synonyms:Benzoicacid, thio-, S-[2-(diethylamino)ethyl] ester (7CI,8CI); Ethanethiol,2-diethylamino-, benzoate (6CI); 2-(Diethylamino)ethanethiol benzoate; NSC229050

Chemical Property of S-[2-(diethylamino)ethyl] benzenecarbothioate

Chemical Property:

• Vapor Pressure: 0.000417mmHg at 25°C
• Boiling Point: 316.2°Cat760mmHg
• Flash Point: 145°C
• Density: 1.056g/cm³

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of S-[2-(diethylamino)ethyl] benzenecarbothioate

There total 4 articles about S-[2-(diethylamino)ethyl] benzenecarbothioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

thiobenzoic acid O-(2-diethylamino-ethyl ester) (3817-58-1) → diethylaminoethylthio benzoate (14441-55-5)

Guidance literature:

at 138 ℃; under 2 Torr;

DOI:10.1016/S0040-4039(01)99531-0

Reference yield:

2-(Diethylamino)ethanol (100-37-8) → diethylaminoethylthio benzoate (14441-55-5)

Guidance literature:

Multi-step reaction with 2 steps

1: chloroform; SOCl₂

2: ethanol

With thionyl chloride; ethanol; chloroform;

Reference yield:

thiobenzoic acid potassium salt (28170-13-0) + 2-(diethylamino)ethyl chloride (100-35-6) → diethylaminoethylthio benzoate (14441-55-5)

Guidance literature:

With ethanol;

upstream raw materials:

thiobenzoic acid potassium salt

2-(diethylamino)ethyl chloride

thiobenzoic acid O-(2-diethylamino-ethyl ester)

2-(Diethylamino)ethanol

Downstream raw materials:

bis(2-(N,N-diethylamino)ethyl)sulfide

2-(diethylamine)ethanethiol

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