4-Chloro-2,3-dimethylpyridine 1-oxide

Base Information

Chemical Name:4-Chloro-2,3-dimethylpyridine 1-oxide
CAS No.:59886-90-7
Molecular Formula:C7H8ClNO
Molecular Weight:157.6
Hs Code.:29333990
European Community (EC) Number:611-910-8
NSC Number:275262
Nikkaji Number:J1.632.223G
Wikidata:Q72449607
Mol file:59886-90-7.mol

Synonyms:59886-90-7;4-CHLORO-2,3-DIMETHYLPYRIDINE 1-OXIDE;4-chloro-2,3-dimethylpyridine n-oxide;4-Chloro-2,3-dimethylpyridine-N-oxide;4-Chloro-2,3-dimethyl-pyridine 1-oxide;4-Chloro-2,3-dimethyl-1-oxidopyridin-1-ium;Pyridine, 4-chloro-2,3-dimethyl-, 1-oxide;4-Chloro-2,3-dimethylpyridine1-oxide;2,3-DIMETHYL-4-CHLOROPYRIDINEN-OXIDE;2,3-Dimethyl-4-chloropyridine N-oxide;2,3-DIMETHYL 4-CHLORO PYRIDINE N-OXIDE;4-chloro-2,3-dimethylpyridin-1-ium-1-olate;SCHEMBL712432;MCUYHRNUDDANSO-UHFFFAOYSA-N;AMY14652;BCP14823;MFCD06411125;NSC275262;4-chlor-2,3-dimethylpyridine-N-oxide;AKOS006293605;4-chlor-2,3-dimethylpyridine-1-oxide;NSC-275262;SB37866;2,3-Dimethyl-4-chloropyridine 1-oxide;2,3-dimethyl-4-chloro-pyridine N-oxide;201605-38-1;AC-15813;AS-10877;A8397;C2820;FT-0602429;EC 611-910-8;4-chloro-2,3-dimethyl-1-oxidopyridin-1-ium =;EN300-1068098;J-514920;4-chloro-2,3-dimethylpyridine 1-oxide

Suppliers and Price of 4-Chloro-2,3-dimethylpyridine 1-oxide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Usbiological
4-Chloro-2,3-dimethylpyridine N-oxide
5g
$ 326.00

TRC
4-Chloro-2,3-dimethylpyridine N-Oxide
25g
$ 140.00

TRC
4-Chloro-2,3-dimethylpyridine N-Oxide
5g
$ 75.00

TCI Chemical
4-Chloro-2,3-dimethylpyridine N-Oxide >98.0%(GC)(T)
5g
$ 58.00

TCI Chemical
4-Chloro-2,3-dimethylpyridine N-Oxide >98.0%(GC)(T)
25g
$ 201.00

SynQuest Laboratories
4-Chloro-2,3-dimethylpyridine N-oxide
25 g
$ 245.00

SynQuest Laboratories
4-Chloro-2,3-dimethylpyridine N-oxide
1 g
$ 45.00

SynQuest Laboratories
4-Chloro-2,3-dimethylpyridine N-oxide
250 mg
$ 25.00

SynQuest Laboratories
4-Chloro-2,3-dimethylpyridine N-oxide
5 g
$ 105.00

Sigma-Aldrich
4-CHLORO-2,3-DIMETHYLPYRIDINE 1-OXIDE Aldrich
1ea
$ 115.00

Total 90 raw suppliers

Chemical Property of 4-Chloro-2,3-dimethylpyridine 1-oxide

Chemical Property:

Appearance/Colour:Pale Yellow Solid
Vapor Pressure:0mmHg at 25°C
Melting Point:103-105 °C
Refractive Index:1.537
Boiling Point:338.459 °C at 760 mmHg
PKA:1.28±0.10(Predicted)
Flash Point:158.495 °C
PSA：25.46000
Density:1.192 g/cm³
LogP:2.38530
Storage Temp.:Room temperature.
Solubility.:Chloroform (Slightly), Methanol (Slightly)
XLogP3:1.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:0
Exact Mass:157.0294416
Heavy Atom Count:10
Complexity:120

Purity/Quality:

99% ^*data from raw suppliers

4-Chloro-2,3-dimethylpyridine N-oxide ^*data from reagent suppliers

Safty Information:

Pictogram(s): Xn
Hazard Codes:Xn
Safety Statements: 24/25

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=C(C=C[N+](=C1C)[O-])Cl
Uses An intermediate in the synthesis of rabeprazole (R070500).

Technology Process of 4-Chloro-2,3-dimethylpyridine 1-oxide

There total 5 articles about 4-Chloro-2,3-dimethylpyridine 1-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 37699-43-7
2,3-dimethyl-4-nitropyridine N-oxide

: 59886-90-7
4-chloro-2,3-dimethylpyridine-N-oxide

Guidance literature:: With acetyl chloride; In ethanol; at 65 ℃; for 5h;

Reference yield: 96.0%

: 37699-43-7
2,3-dimethyl-4-nitropyridine N-oxide

: 75-36-5
acetyl chloride

: 59886-90-7
4-chloro-2,3-dimethylpyridine-N-oxide

Guidance literature:: 2,3-dimethyl-4-nitropyridine N-oxide; acetyl chloride; In ethanol; at 65 ℃; Large scale reaction;

With sodium hydroxide; In ethanol; water; toluene; pH=7.5 - 8.5; Large scale reaction;
DOI:10.1021/op9003357

Reference yield: 49.0%

: 22710-07-2,166521-76-2
2,3-dimethylpyridine 1-oxide

: 59886-90-7
4-chloro-2,3-dimethylpyridine-N-oxide

Guidance literature:: 2,3-dimethylpyridine 1-oxide; With chlorine; In dichloromethane; at 25 ℃; for 1.5h; Green chemistry;

With sodium hydroxide; In dichloromethane; at 25 ℃; Green chemistry;
DOI:10.13005/ojc/330244