4-chloro-N'-(2-furylmethylene)benzohydrazide

Base Information

Chemical Name:4-chloro-N'-(2-furylmethylene)benzohydrazide
CAS No.:93418-01-0
Molecular Formula:C₁₂H₉ClN₂O₂
Molecular Weight:248.669
Hs Code.:
European Community (EC) Number:660-096-0
NSC Number:216994
DSSTox Substance ID:DTXSID30425388
ChEMBL ID:CHEMBL485550

Synonyms:NSC216994;93418-01-0;4-chloro-N'-(2-furylmethylene)benzohydrazide;4-chloro-N'-(furan-2-ylmethylene)benzohydrazide;CHEMBL485550;SCHEMBL8291227;DTXSID30425388;STK236055;AKOS001299410;NSC-216994;SR-01000107757;SR-01000107757-1;Z49577948;4-chloro-N'-[(E)-furan-2-ylmethylidene]benzohydrazide

Suppliers and Price of 4-chloro-N'-(2-furylmethylene)benzohydrazide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of 4-chloro-N'-(2-furylmethylene)benzohydrazide

Chemical Property:

Boiling Point:°Cat760mmHg
Flash Point:°C
Density:1.29g/cm³
XLogP3:2.9
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:3
Exact Mass:248.0352552
Heavy Atom Count:17
Complexity:288

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=COC(=C1)C=NNC(=O)C2=CC=C(C=C2)Cl
Isomeric SMILES:C1=COC(=C1)/C=N/NC(=O)C2=CC=C(C=C2)Cl

Technology Process of 4-chloro-N'-(2-furylmethylene)benzohydrazide

There total 2 articles about 4-chloro-N'-(2-furylmethylene)benzohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 98-01-1
furfural

: 536-40-3
4-chlorobenzoic acid hydrazide

: 93418-01-0
4-chloro-N'-(furan-2-ylmethylene)benzohydrazide

Guidance literature:: In ethanol; for 3h; Reflux;
DOI:10.1039/b811612a

Reference yield:

: 98-01-1
furfural

: 536-40-3
4-chlorobenzoic acid hydrazide

: 93418-01-0
furfural-(4-chloro-benzoylhydrazone)

Guidance literature:

Reference yield: 90.0%

: 93418-01-0
4-chloro-N'-(furan-2-ylmethylene)benzohydrazide

: 7550-45-0
titanium tetrachloride

: 102136-87-8
{TiCl₂(C₆H₄ClCONNCHC₄H₃O)2}

Guidance literature:: In chloroform; 1 equiv. of TiCl4 and 2 equivs. of hydrazone were refluxed for 1 h;; the precipitate was removed by filtration, washed with CHCl3 and Et2O and dried in vacuo; elem. anal.;;
DOI:10.1016/S0020-1693(00)85666-2